VOC analysis results, sample AE10240, May 3, 2002

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Data File C:\MSDCHEM\l\5973N\02MAY03\10516.D Vial: 21 Acq On 4 May 2002 1:41 am Operator: Sample nyc Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSC.P Quant Method : C:\MSDCHEM\1...\W050302.M (RTE Integrator) Title : VOC method 8260 Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 3 7-Oxabicyclo[4.1.0]heptane Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

30.50 0.03 ug/L 18894 1,4-Dichlorobenzene-d4 31.54

Hit#.of 5 Tentative ID MW MolForm CAS# Qual

1 7-Oxabicycro[4.1.0]heptane 98 C6H10O 000286-20-4 47 2 Decanal (CAS) $$ n-Decanal $$ De... 156 C10H20O 000112-31-2 40 3 1,6;3', 4-Dianhydro-2-deoxy-.beta. . . . 128 C6H8O3 050767-53-8 35 4 1-Nonanol (CAS) $$ n-Nonyl. alcoh... 144 C9H20O 000143-08-8 25 Abundance Scan 2701 (30.497 min): 10516.D (-) m/z SYTTO 100.00% 5)7

43 5000 70 83 I I 50 79 98 30.20 30,40 30,60 30.80 0 '' I'''' I' ‘ I m/z55700 59.71% m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance , #7213; 7-Oxabicyclo[4.1.0]heptane 41 83

27 54 5000 ' ' I ' ' 30.20 30.40 30.60 30.80 70 m/z43.10 51.00% 97 0 ll.M.... mZz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #55838: Decanal (CAS) $$ n-Decanal $$ Decyl aldehyde $$ De... 4)3 517 MX30.20 30.40 30.60 30.80 5000 ■m/z 44.00 42.14% 70

0 I' ‘ ‘ ‘ I *' ‘ ‘ I'''' I' ‘‘ I p-n-rp-r ' ' I ‘ ' I ' ' I'' *' I''' ' I''' ‘ I ‘' I''' ‘ I Tife-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #24119; 1.6;3,4-Dianhydro-2-deoxy-.beta.-d-lixo-hexopyranose 44 57 83 30.20 30,40 30.60 30.80 m/z 56.10 33.00% 5000 72

■n/z~> 0 '' I'''' I'''' I'''' I'''' I T-rp-r 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 "I''''I‘' ''I''‘ 'I ' ' I ' ' ‘ ' I 11 30.20 30.40 30.60 30.80

10516.D W050302.M Mon May 06 10:32:35 2002 Page 5 .

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