VOC analysis results, sample AE09569, April 26, 2002

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Data File C:\MSDCHEM\l\5973N\02APR26\0426Bl.D Vial: 1 Acq On 26 Apr 2002 8:58 am Operator: Sample lb Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\W042302 .M (RTE Integrator) Title : VOC method 8260 Library- : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 5 .beta.-phenylpropyl isothio... Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T.

33.72 0.07 ug/L 37798 1,4-Dichlorobenzene-d4 31.54 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 .beta.-phenylpropyl isothiocyanate 177 ClOHllNS 000000-00-0 38 2 Hydroperoxide, 1-methyl-1-phenyl... 152 C9H12O2 000080-15-9 35 3 Benzenepropanenitrile, .beta.-oxo- 145 C9H7NO 000614-16-4 27 4 benzophenone 120 C8H8O 000000-00-0 27 Abundance Scan 3028 (33.724 min): 0426B1 .D (-) m/z 105.00 100.00% 4(3 Ids 77 121

5000 91 A A 12 65 209 33.40 33.60 33.80 34.00 0^ I'''' 1 m/z 43.05 98.01% Tl/Z~> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 Abundance #82123: .beta.-phenylpropyl isothiocyanate 1(1)5 118 80 ........................... 552 33.40 33.60 33.80 34.00 m/z 77.00 79.32% 95 I I 177 ■nfe~> Qi A I'''' I 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 Abundance #48984: Hydroperoxide, 1-methyl-1-phenylethyl $$ Hydropero... 43 105 33.40 33.60 33.80 34.00 5000 77 121 m/z 121.10 67.46% 51

oi ItTTTT ■n/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 Abundance #41369: Benzenepropanenitrile, .beta.-oxo- T' ' '1 1(115 33.40 33.60 33.80 34.00 77 “niTz 4^705 50.00% 118 5000 51 90 145 0 4—t A I'''' I J ' ''' ' T T)ZZ~> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 33.40 33.60 3380 34.00

0426B1.D W042302.M Tue Apr 30 11:46:42 2002 Page 7

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