11.1 Reference Methods
11.1.1 The Environmental Protection Agency (EPA) Information Collection Rule (ICR)
Microbial Laboratory Manual, April 1996
11.1.2 The EPA Method 1623, April 1999.
12 Quality Assurance and Quality Control (QA/QC) Checks
12.1 Confmnation and verification of presumed oocysts and/or cysts are perfonned by
making comparison to the positive and negative control organisms examined with
each sample. Cysts and oocysts are only "confinned" if internal stnictures are
identified.
12.2 As a sterility indicator, the temperature is checked during autoclaving runs to
make sure appropriate sterilization temperatures are being attained. This is
maintained in the logbook that is kept near the autoclave. The accurateness of the
autoclave is checked by autoclave tape, kill-it ampules, broth tests and
temperature checks. These results are recorded in a logbook located next to the
autoclave.
12.3 Over the course of a week, all of the samples processed using the ICR method are
considered a BATCH. A negative and a positive filter are processed as QC
samples for each batch for each week. These filters are prepared according to the
instructions in the ICR for QC samples. Matrix spikes are perfoiTned weekly and
matrix spike duplicates are perfonned monthly.
12.4 Over the course of a week, all of the samples processed using the 1623 method
ai’e considered a BATCH. A negative and a positive filter are processed as QC
samples for each batch for each week. These filters are prepared according to the
instructions in the 1623 manual for QC samples. Matrix spikes are perfonned
weekly.
12.5 The PE samples are cunently distributed by the US EPA, since NYC DEP is part
of the National Performance Evaluation Program.
12.6 Deviation in microscopic counts between analysts is derived from duplicate
counts perfonned by each Principle Analyst quarterly.
13 QC Summary
13.1 Documentation
QUAL1080D02.doc
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NYC-WTC_000072141
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NYC-WTC_000072141Source: NYC Law Department, mirrored locally
Document containing editorial comments and requirements regarding trigger mechanisms, clearance levels, and supervision for the residential cleaning scope of work.
Document containing editorial comments and requirements regarding trigger mechanisms, clearance levels, and supervision for the residential cleaning scope of work.