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GCMS analysis results for sample AD24981, Nov 2001

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Laboratory report documenting GCMS analysis of sample AD24981 conducted on November 19, 2001, identifying unknown compounds.

NYC-WTC_000069193–000069203

Folder label: “GCMS Scan X 10/19/01 An 11/8/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File C:\HPCHEM\1\DATA\NOVO 8O1\24981.D Vial: 10 Acq On 8 Nov 2001 11:24 pm Operator; 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering; 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs; 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 7.686 284 288 307 rBV 155642 456853 7.04% 1.344% 2 11.578 707 712 721 rBV 46289 114089 1.76% 0.336% 3 11.707 721 726 744 rBV 1709551 4446962 68.49% 13.078% 4 15.315 1113 1119 1138 rBV 2700459 6044364 93.10% 17.776% 5 20.593 1688 1694 1713 rBV 2959438 6492514 100.00% 19.094%

6 25.018 2169 2176 2188 rBV2 2751399 6037299 92.99% 17.755% 7 33.060 3044 3052 3074 rBV2 2265701 5383233 82.91% 15.832% 8 37.164 3490 3499 3523 rBV2 1718072 5027876 77.44% 14.786%

Sum of corrected areas: 34003190 24981.D NP103001.M Mon Nov 19 12:13:09 2001

NYC-WTC_000069199

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NYC-WTC_000069199Source: NYC Law Department, mirrored locally

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