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GCMS analysis results for sample AD24476, Nov 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD24476 conducted on November 14, 2001, identifying unknown compounds.

NYC-WTC_000068485–000068495

Folder label: “GCMS Scan X 10/12/01 An 11/3/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File C:\HPCHEM\1\DATA\NOV0 201\24476.D Vial; 12 Acq On 3 Nov 2001 1:44 am Operator; 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing ; OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation; 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 7.692 285 288 294 rBV 84759 194743 4.13% 0.786% 2 11.575 707 711 720 rBV 36839 85689 1.82% 0.346% 3 11.713 720 726 746 rBV 1317535 3326806 70.54% 13.421% 4 15.321 1113 1119 1138 rBV 2044626 4514795 95.73% 18.214% 5 20.599 1687 1694 1711 rBV 2144765 4716280 100.00% 19.027%

6 25.024 2169 2176 2187 rBV 2063921 4521332 95.87% 18.240% 7 33.057 3044 3051 3076 rBV2 1720223 4033614 85.53% 16.273% 8 37.161 3489 3498 3518 rBV2 1175333 3394171 71.97% 13.693%

Sum of corrected areas: 24787430

24476.D NP103001.M Tue Nov 13 10:09:30 2001

NYC-WTC_000068491

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NYC-WTC_000068491Source: NYC Law Department, mirrored locally

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