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Document / 28 pages

GC/MS calibration table for TCLP analysis, Nov 2001

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Document containing tabular laboratory data including pH and count metrics for environmental sample analysis in November 2001.

NYC-WTC_000069154–000069181

Folder label: “GCMS Scan X 10/19/01 An 11/8/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\NOV0801\LBA.D Vial: 8 Acq On : 8 Nov 2001 9:26 pm Operator: 209 GALOS Sample : 10/19 lab blk Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 6.427 147 151 162 rVV2 46783 127209 1.32% 0.172% 2 7.685 285 288 306 rBV 141047 385868 4.00% 0.523% 3 11.568 707 711 721 rBV 75735 187107 1.94% 0.253% 4 11.706 721 726 749 rW 2533390 6655515 68.93% 9.013% 5 15.323 1113 1120 1137 rBV 4099417 8974204 92.94% 12.153% 6 20.602 1688 1695 1714 rBV 4334802 9655838 100.00% 13.076% 7 25.027 2169 2177 2189 rBV2 4051522 9080347 94.04% 12.297% 8 27.267 2416 2421 2427 rVB 74478 142683 1.48% 0.193% 9 29.452 2653 2659 2667 rBV 1470694 2864895 29.67% 3.880% 10 29.562 2667 2671 2681 rW 386467 838052 8.68% 1.135% 11 29.699 2681 2686 2699 rVB 249435 527190 5.46% 0.714% 12 30.645 2783 2789 2801 rBV 640588 1277846 13.23% 1.731% 13 31.591 2886 2892 2897 rBV 1087453 2286689 23.68% 3.097% 14 31.682 2897 2902 2912 rW 1157559 2481713 25.70% 3.361% 15 31.811 2912 2916 2927 rVB 93339 228178 2.36% 0.309% 16 32.674 3004 3010 3022 rBV 1132546 2491442 25.80% 3.374% 17 33.069 3044 3053 3070 rBV2 3368398 8423443 87.24% 11.407% 18 33.629 3103 3114 3136 rBV 1257130 2869426 29.72% 3.886% 19 34.556 3210 3215 3230 rBV 925496 2065288 21.39% 2.797% 20 35.446 3306 3312 3324 rBV 728552 1752506 18.15% 2.373% 21 35.602 3324 3329 3338 rVB2 29903 105277 1.09% 0.143% 22 36.300 3399 3405 3427 rBV 378809 1104868 11.44% 1.496% 23 36.750 3447 3454 3462 rBV 34169 126537 1.31% 0.171% 24 37.172 3490 3500 3505 rBV2 2573534 7807991 80.86% 10.574% 25 38.063 3589 3597 3614 rVB 37972 164065 1.70% 0.222% 26 38 .283 3615 3621 3628 rBV2 70269 256817 2.66% 0.348% 27 39.513 3747 3755 3761 rBV4 38421 167795 1.74% 0.227% 28 39.633 3762 3768 3781 rVB5 41787 225595 2.34% 0.306% 29 41.579 3969 3980 3997 rBV4 34293 240338 2.49% 0.325% 30 44.030 4235 4247 4257 rBV3 25305 190133 1.97% 0.257% 31 47.142 4567 4586 4590 rBV8 18594 136609 1.41% 0.185%

NYC-WTC_000069158

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NYC-WTC_000069158Source: NYC Law Department, mirrored locally

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