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GCMS calibration table for TCLP method, Nov 2001

Machine-extracted title · confidence 100%

Calibration record for GC/MS instrument using TCLP method, listing standard compounds and response data from November 6, 2001.

NYC-WTC_000069030–000069039

Folder label: “GCMS Scan X 10/18/01 An 11/6/01

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Scanned page image, NYC-WTC_000069034
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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C:\HPCHEM\1\DATA\NOV0601\LBA.D Vial: 9 Acq On : 6 Nov 2001 8:36 pm Operator: 209 GALOS Sample : lb 10/18 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 6.314 134 138 144 rBV 35168 71671 1.23% 0.229% 2 6.424 146 150 160 rW2 49678 136144 2.33% 0.436% 3 6.662 173 176 182 rBV 38241 76533 1.31% 0.245% 4 7.681 283 287 312 rBV 357126 962189 16.47% 3.078% 5 11.574 705 711 720 rBV 44016 110932 1.90% 0.355% 6 11.712 720 726 750 rW 1607853 4011700 68.67% 12.833% 7 15.319 1113 1119 1136 rBV 2585583 5441827 93.15% 17.408% 8 20.598 1687 1694 1712 rBV 2772486 5842180 100.00% 18.689% 9 25.023 2169 2176 2188 rBV2 2603937 5705185 97.66% 18.251% 10 33.065 3042 3052 3070 rBV2 2028446 4919730 84.21% 15.738% 11 37.159 3490 3498 3520 rBV2 1372457 3982029 68.16% 12.738%

Sum of corrected areas; 31260120 LBA.D NP103001.M Fri Nov 16 11:58:03 2001

NYC-WTC_000069034

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NYC-WTC_000069034Source: NYC Law Department, mirrored locally

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