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GCMS calibration table for TCLP analysis, Nov 2001

Machine-extracted title · confidence 90%

Calibration data table for GC/MS instrument used in TCLP analysis, generated on November 5, 2001.

NYC-WTC_000068559–000068571

Folder label: “508 Scan X 10/16/01 A 11/5/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C:\HPCHEM\1\DATA\NOV0501\LB.D Vial: 2 Acq On : 5 Nov 2001 12:14 pm Operator: 209 GALOS Sample : 10/16 lab blk Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge <100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 6.327 136 140 146 rBV 36513 73597 1.38% 0.266% 2 6.428 148 151 162 rVV2 51741 137218 2.57% 0.495% 3 6.566'1^ 162 166 174 rW 27228 64622 1.21% 0.233% 4 6.676 174 178 187 rVB 35201 79598 1.49% 0.287% 5 7.163 226 231 238 rBV 29121 106309 1.99% 0.384%

6 7.695 285 289 302 rBV 113104 276079 5.17% 0.996% 7 11.569 707 711 721 rBV 38827 94581 1.77% 0.341% 11.707^, 721 726 745 rBV 1443665 3570649 66.81% 12.881% 15.315^ 1113 1119 1135 rBV 2240163 4865902 91.04% 17.554% / 10 20.603'*« 1688 1695 1713 rBV 2371488 5344729 100.00% 19.282% f ■ 11 25.028 2170 2177 2189 rBV2 2283371 5204599 97.38% 18.776% , 12 33.060x 3045 3052 3073 rBV2 1850048 4356350 81.51% 15.716% I 13 37.164\ 3491 3499 3519 rBV2 1281571 3545228 66.33% 12.790%

Sum of corrected areas: 27719461 LB.D NP103001.M Fri Nov 09 12:14:06 2001

NYC-WTC_000068563

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NYC-WTC_000068563Source: NYC Law Department, mirrored locally

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