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← Document results/DEP Box 67/GC/MS Scan 9/26/01
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GC/MS calibration table for TCLP analysis, Oct 18 2001

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Calibration data table for TCLP analysis using GC/MS standards processed on October 18, 2001.

NYC-WTC_000088491–000088503

Folder label: “GC/MS Scan 9/26/01”

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C:\HPCHEM\1\DATA\OCT1801\LB.D Vial: 2 Acq On : 18 Oct 2001 5:09 pm Operator: 209 GALOS Sample : lab blk 10/15 Inst ; GC/MS 209 Mise Multiplr: 1.00 MS Integration Params-. LSCINT.P Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 6.368 140 145 151 rBV 21084 45805 1.70% 0.319% 2 6.479 151 157 168 rW 36844 103630 3.86% 0.721% 3 6.616 168 172 18 0 rW 18519 45594 1.70% 0.317% 4 6.726 180 184 194 rVB 24905 57269 2.13% 0.399% 5 7.745 292 295 306 rBV 42582 110640 4.12% 0.770% 6 11.629 713 718 727 rBV2 21420 49498 1.84% 0.344% 7 11.766 727 733 748 rBV 766888 1945548 72.41% 13.539% 8 15.374 1120 1126 1143 rBV 1237068 2632307 97.97% 18.318% 9 20.653 1695 1701 1712 rBV 1208826 2686735 100.00% 18.697% 10 25.087 2177 2184 2195 rBV2 1142469 2515841 93.64% 17.507%

11 33.120 3052 3059 3082 rBV2 955535 2261711 84.18% 15.739% 12 37.233 3496 3507 3522 rBV2 667298 1915630 71.30% 13.331%

Sum of corrected areas: 14370208 LB.D NP091101.M Fri Oct 19 10:25:29 2001

NYC-WTC_000088495

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NYC-WTC_000088495Source: NYC Law Department, mirrored locally

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