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GCMS analysis results, sample AD23993, Oct 2001

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DEP lab report for GCMS analysis of sample AD23993 conducted on October 25, 2001, noting unknown compounds.

NYC-WTC_000067690–000067704

Folder label: “GCMS Scan X 10/4/01 An 10/18/01

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NYC 9/11 Public Portal Document

Library Search. Compound Report Data File : C:\HPCHEM\1\DATA\OCT1701\23948.D Vial: 15 Acq On : 18 Oct 2001 2:58 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Hexanone Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 6.39 0.46 ug/1 43452 1,4-Dichlorobenzene-d4 11.77 Hit# of 5 Tentative ID MW MolForra CAS# Qual 1 3-Hexanone 100 C6H12O 000589-38-8 58 2 3-Pentajione, 2-methyl- 100 C6H12O 000565-69-5 40 3 2,4-Peiitanedione 100 C5H8O2 000123-54-6 35 4 Hexat^cane 226 C16H34 000544-76-3 28 Abundance ' Scan 147 (6.386 min): 23948.D (-) m/z 43.00 100.00% 4|3 57

71 5000 100

6.00 6.20 6,40 6.^ 6.80 tprrTTpTTTT m/z 57.00 89717% ■nfe-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1528:3-Hexanone 43 57

29 71 5000 6.00 6.20 6.40 6.60 6.80 100 m/z 71.00 64.58% (I

JLJku +t +TTrpTTTJ- 'nfe-> 202530^ 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63398:3-Pentanone. 2-m8thyl- 5|7 43 6,00 6,20 6.40 6.^ 6.80 5000 m/z 100.05 39.16% 100 71

+pTTTpTTp+ 85 Tife-> Abundance 20253035404550556065 70 75 80859095 100105

43 #63324:2.4-Pentanedione k....... 6.00 6.20 6.40 __________ 6.60 6.80 “mTz 41.05 33.70% 5000

nfe-> 58 +7-rTTTyTrTT|TT+T7rTTT^^ 72 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 85 100

T JjM 6.00 6.^ 6.^ aro 6.M

23948.D NP101901.M Wed Oct 24 11:21:55 2001 Page 1

NYC-WTC_000067698

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NYC-WTC_000067698Source: NYC Law Department, mirrored locally

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