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GCMS analysis results, sample AD23903, Oct 2001

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DEP lab report for GCMS analysis of sample AD23903 conducted on October 23, 2001, noting unknown compounds.

NYC-WTC_000067495–000067507

Folder label: “GCMS Scan X 10/2/01 An 10/17/01

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NYC 9/11 Public Portal Document

Library Search Confound Report Data File : C:\HPC3IEM\1\DATA\OCT1701\23903.D Vial: 8 Acq On : 17 Oct 2001 8:09 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Hexanol Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 6.74 0.47 ug/1 48285 1,4-Dichlorobenzene-d4 11.76 Hit# of 5 Tent ve ID MW MolForm CAS# Qual 1 2-Hexanol 102 C6H14O 000626-93-7 83 x61, 4-methyl- 2 2-Pentar^ 102 C6H14O 000108-11-2 74 3 2-He: Ihol, (R)- 102 C6H14O 026549-24-6 43 4 2- ntanol, 3-methyl -______________ 102 C6H14O 000565-60-6 39 Abunddice Scan 185 (6.736 min): 23903.D (-) m/z 44.95 100.00% 4)5

5000

69 I . 1 .-T . ■' P ' 41 8487 6.40 6.60 6.% 7.00 .. m/z 69.00 16.84% TiZz-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Sibundance #63584:2-Hexanol 4)5

a 5000 6.40 6.60 6.80 7.00 69 “mTz 41.05 15.55% ..... FS....... I........ ......... mfe-> Abundance 10 15 20253035404550556065 70 75 8085 90 95 #63545:2-Pentanol, 4^nethyl- 4)5 jvWL^ 6.40 6.60 6.80 7.00 5000 m/z 43.05 12.41% 69 27 57 I 8487 "" I"' ‘ 111" I" "I"' 11" " I' ■" 1 ■" 11' I" I" • • 11 n4->10 J5 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #1794:2-Hexanol, (R)- T T 4)5 6.^ iro' 6.^ 7.00 m/z 44.00 8.90% 5000

29 69 19 ^42 , 55 I 8487 m/z-> 6.40 6.60 6.80 7.00

23903.D NP101901.M Tue Oct 23 12:49:43 2001 Page 2

NYC-WTC_000067504

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NYC-WTC_000067504Source: NYC Law Department, mirrored locally

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