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Pesticide reference standard analysis, sample AD22582, Sept 2001

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Reference standard testing results for pesticide analysis of sample AD22582, verifying analytical method performance with known compounds.

NYC-WTC_000063290–000063355

Folder label: “525 9/24/01 EX 9/29 - 9/30 Analysis”

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Integration Report Quanfile: C2CC929 Quan Entries: 28 Comment: BOHLK; METHOD 525; INST 204; 09/29/01; C2 Sorted uia: Entry Number t

No Name of Gonpound R Time Scan# Mode Peak Ar^a PR Height 3 chrysene d-12(IS) 22:57 1377 Auto 2,605,336 1,011,873 4 p-terphenyl d-14(IS) 21:01 1261 Auto 3,787,048 2,659,745 5 acenaphthene d-10(SURR 12:32 752 Auto 2,658,960 1,885,593 6 phenanthrene d-10(SURR 17:16 1036 Auto 3,863,002 1,736,363 7 chrysene d-12 (SURR) 22:57 1377 Auto 2,605,336 1,011,873 8 1,3-d imethy1-2-n itrobe 8:12 492 Auto 1,639,012 876,027 9 triphenyl phosphate (S 22:19 1339 Auto 1,758,042 825,369 10 perylene d-12 (SURR) 27:30 1650 Auto 1,644,334 350,404 11 hexachlorocyclopentad i 10:23 623 Auto 6,243 3,895 12 hexachlorobenzene 15:42 942 Auto 27,587 11,061 13 simazine 16:28 988 Auto 12,641 4,116 14 atrazine 16:40 1000 Auto 10,512 4,631 15 alachlor 18:37 1117 Auto 27,426 15,228 16 bis(2-ethyIhexy1)adipa 22:11 1331 Auto 53,895 12,475 17 b is(2-ethyIhexy1)phtha 23:14 1394 Auto 98,862 20,733 18 benzo C a)pyrene 27:15 1635 Auto 53,293 7,274 19 eptc 10:47 647 Auto 147,511 78,945 20 2,6—d in itrotoluene 12:09 729 Auto 17,082 9,095 21 2,4-d in itrotoluene 13:09 789 Auto 18,323 5,915 22 molinate 13:17 797 Auto 49,841 30,787 23 terbac i1 17:36 1056 Auto 5,980 2,512 c o 24 acetochlor 18:26 1106 Auto 18,724 10,548 E3 25 metribuzin 18:28 1108 Auto 28,155 15,180 o o 26 metolachlor 19:21 1161 Auto 77,16© 37,097 Q 27 butachlor 20:34 1234 Auto TO 30,050 11,384 ■c o 28 4,4'-dde 20:57 1257 Auto 41,734 29,858 co co Q_ <D O .0 o Z3 o o 0. o'

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