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Pesticide reference standard analysis, sample AD22582, Sept 2001

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Reference standard testing results for pesticide analysis of sample AD22582, verifying analytical method performance with known compounds.

NYC-WTC_000063290–000063355

Folder label: “525 9/24/01 EX 9/29 - 9/30 Analysis”

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Quantitation Report Quanfile: C2CC929 Quan Entries: 28 Comment: ROHLK; METHOD 525; INST 204; 09/29/01; C2 Sorted via: Entry Number t (S) = Standard

Cal Name of Compound S Scan# R Time Me Calc f^rntCA) Units

3 chrysene d-12CIS) I 1377 22:57 RR 5.000 UG/L 4 p-terphenyl d-14CIS) I 1261 21:01 RR 5.000 UG/L 5 acenaphthene d-10CSURR A 752 12:32 RR 5.147 UG/L 6 phenanthrene d-10CSURR A 1036 17:16 RU 4.971 UG/L 7 chrysene d-12 (SURR) A 1377 22:57 RR 4.881 UG/L 8 1,3-d imethy1-2-n itrobe A 492 8:12 RR 5.020 UG/L 9 triphenyl phosphate (S A 1339 22:19 RR 4.886 UG/L 10 perylene d-12 CSURR) A 1650 27:30 RR 5.501 UG/L 11 hexachlorocyclopentad i A 623 10:23 RR 0.081 UG/L 12 hexachlorobenzene A 942 15:42 RR 0.095 UG/L 13 simazine A 988 16:28 RR 0.088 UG/L 14 atrazine A 1000 16:40 RR 0.085 UG/L 15 alachlor A 1117 18:37 RR 0.116 UG/L 16 bis(2-ethyIhexy1)adipa A 1331 22:11 MM 0.123 UG/L 17 b is(2-ethyIhexy1)phtha A 1394 23:14 RR 0.127 UG/L 18 benzo(a)pyrene A 1635 27:15 MM 0.117 UG/L 19 eptc A 647 10:47 MM 0.093 UG/L 20 2,6-d ini troto1uene A 729 12:09 RR 0.089 UG/L 21 2,4-d in itrotoluene A 789 13:09 RR 0.076 UG/L 22 molinate A 797 13:17 RR 0.092 UG/L 23 terbacil A 1056 17:36 RR 0.080 UG/L c o 24 acetochlor A 1106 18:26 RR 0.109 UG/L E3 25 metribuzin A 1108 18:28 RR ,0.112 UG/L o 26 metolachlor A 1161 19:21 RR 0.115 UG/L o Q 27 butachlor A 1234 20:34 MM 0.119 UG/L CM TO ■d o 28 4.4"-dde A 1257 20:57 RR 0.119 UG/L co co CL CO o O o z3 o CL 5 a o s 0 z z

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NYC-WTC_000063352Source: NYC Law Department, mirrored locally

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