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GC/MS blank analysis results, April 17 2002

Machine-extracted title · confidence 100%

Laboratory report showing GC/MS blank analysis for Method 508 compounds with non-detectable levels.

NYC-WTC_000060438–000060445

Folder label: “GCMS X 3/21/02 A 4/16/02

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Scanned page image, NYC-WTC_000060444
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\APR1602\LB.D Vial: 3 Acg On : 16 Apr 2002 3:02 pm Operator: Sample : gc/ms scan 3/22 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TGLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3,4-Dihydroxybenzyl alcohol,tr Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. 14.82 2.06 ug/1 390743 Naphthalene-d8 15.84

Hit# of Tentative ID. 5 MW MolForm CAS# Qual J___________ 1 3,4-Dihydroxybenzyl alcohol,tris(tr 356 C16H32O3Si3 068595-79-9 70 2 Palmitic acid, 2-(trimethylsiloxy)e 372 C21H44O3Si 022613-62-3 53 ^3 Cyclopentasyloxane, decamethyl- 370 C10H3005Si5 000541-02-6 53 4 Phenethylamine, N-methyl-.beta.,3,4 399 C18H37NO3Si3 010538-85-9 43 Abundance I Scan 1064 {14.816 min): LB.D (-) m/z 73.00 100.00% 73

355 267 5000

T 45 14.40 14.60 14.80 15.00 15.20 I I m/z 355.05 61.08% !,&-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #49868: 3,4-Dihydroxybenzyl alcohol,tris(trimethylsilyl)- 73

5000 179 267 M 14.40 14.60 14,80 15.00 15.20 356 m/z 267.00 54.25% 45 147

■n/z-> K I' '' ' I I'''' I I ' ' '' I I, 209 237 , I" I"'' I" " I 312 I' ‘' I 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51549: Palmitic acid, 2-(trimethylsiloxy)ethyl ester 713 116 M - 239 14.40 14.60 14.80 15.00 15.20 5000 m/z 356.05 22.02% 176 357 313 I'''' I I I'»' • I' " «I I 330 i " '' I " " I " " I'''' I nfe—> Abundance 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 70 #51266; Cyclopentasiloxane, decamethyl- I 14.40 14.60 14.80 15.00 15.20 m/z 268.00 15.05% 355 267 5000

191207 251 ■n/z-> 40 60 80 10b 120 140 160 180 200 220 240 260 280 300 320 340 360 14.40 14.60 14.80 15.00 15.20

LB.D GCMS0412.M Wed Apr 17 12:04:55 2002 Page 1

NYC-WTC_000060444

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NYC-WTC_000060444Source: NYC Law Department, mirrored locally

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