GCMS analysis results for sample AE07317, April 2002

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Laboratory report documenting GCMS analysis of sample AE07317 conducted on April 10, 2002.

NYC-WTC_000046664–000046672

Folder label: “GCMS X 3/28/02 A 2/27/02”

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Data File C:\HPCHEM\1\DATA\APR0 302\7317.D Vial: 13 Acq On 4 Apr 2002 12:33 am Operator: Sample gc/ms scan 3/28 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0403.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 3,4-Dihydroxybenzyl alcohol,tr Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

14.85 0.98 ug/1 146979 Naphthalene-d8 15.89 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3,4-Dihydroxybenzyl alcohol, tris (tr 356 C16H3203Si3 068595-79-9 53 2 Cyclopentasiloxane, 370 C10H3005Si5 000541-02-6 49 decamethyl- 3 N-(Trifluoroacetyl)-N,O,O',0''-tetr 553 C22H42F3NO4Si4 000000-00-0 47 4 Phenethylamine, N-methyl - . beta . , 3,4 399 C18H37NO3Si3 010538-85-9 43 Abundance Scan 1068 (14.848 min): 7317.D (-) m/z 73.00 100.00% 73

267 355 5000 1 ■ 1 i ■ ■ 45 14.60 14.80 15.00 15.20 125 154 193 223 323 ■ 1 i 1 ' ' ' i ' —————————— m/z 3 55.05 50.35% m/z->_____ 50 100 150 200 250 300 350 400 450 500 550 Abundance #49868: 3,4-Dihydroxybenzyl alcohol,tris(trimethylsilyl)- 73

267 5000 179 14.60 14.80 15.00 15.20 356 45 147 m/z 267.00 49.25% 209 237, 312 — ———— 11 di m/z-> 50 100 1 50 200 250 300 350 400 450 500 550 Abundance #51266: Cyclopentasiloxane, decamethyl- 73 .......... ' 1 ■ 1 i I\............. 1 ' ' 1 i 1 ■ 11 i '' ■ i ■ 355 14.60 14.80 15.00 15.20 267 5000 m/z 356.05 17.19%

207 ■ । । 323. । ■ ■ ■ ■ i ■ • ■ ■ । ■ > ■ ■ । 1 ' । > । ' 1 ■ i ■ - i ■ ■ ■ ■ i • ■ i ■ ■ ■ • ■

m/z->______50 100 150 200 250 300 350 400 450 500 550 Abundance #60162: N-(Trifluoroacetyl)-N,O,O',O"-tetrakis(trimethylsi 1111 73 14.60 14.80 15.00 15.20 m/z 268.00 14.08% 355 5000

45 1 147 193 267 538 ----- 1 1 i 1 ' r i ' 1 ‘ 1 'i 1 ' ' 1 i ' 1 1 ' i 1 ■' 1 ■ i ■ ■ 1 1 I*1 1 1 1 I 1 1 ' ' I 1 ' 1 1 i 1 1 1 1 i 1 1 m/z—> 50 100 150 200 250 300 350 400 450 500 550 14.60 14.80 15.00 15.20

7317.D GCMS0403.M Tue Apr 09 13:08:54 2002 Page 1

NYC-WTC_000046671

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GCMS analysis results for sample AE07316, April 2002 · Box DEP Box 27

NYC-WTC_000046655

Laboratory report documenting GCMS analysis of sample AE07316 conducted on April 10, 2002.

1 shared topics · Same agency, volume and box · similarity 0.998