GCMS analysis results for sample AE06406, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\020409\6406.D Vial: 10 Acq On 9 Apr 2002 11:32 pm Operator: McLean Sample 3/18 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1...\SCANAPR0902.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:'\DATABASE\nist98 .1 ********************************************************************* Peak Number 2 Glycine Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T.

3.52 0.26 ug/1 189677 1,4-Dichlorobenzene-d4 10.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Glycine 75 C2H5NO2 000056-40-6 2 2 Propane, 1,1-dimethoxy- • 104 C5H12O2 004744-10-9 2 3 Hydrazinecarboxamide 75 CH5N3O 000057-56-7 1 4 Glycine 75 C2H5NO2 000056-40-6 1 Abundance Scan 75 (3.520 min): 6406.D (-71) (-) m/z 75.10 100.00% 7)5

5000 40 47

I 3.20 “m/z 3.40 4^700 3.60 3.80 25.14% ■n/z->________ 10 20 30 40 50 60 70 80 90 100 110 Abundance #108147: Glycine 33

553 3.20 3.40 3.60 3.80 m4z40^^^24 790% 57 69 75 ' ' I ' ' ' ' I ' ‘ ■ I ' ' ' ' I ' ' ' ' I ' ■ ' ' I ' ■nfe-> 10 20 30 40 50 60 70 80 90 100 110 <\bundance #28725: Propane, 1,1-dimethoxy- 7&

320 3.40 3.60 3.80 29 m/z 4^70^0 18.35% 5000 45

87 . ....^V7l|l|l, 103 Tl/Z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1072: Hydrazinecarboxamide 3(1 3 20 3.40 3.60 3.80 44 m/z 51.05 1.06% 5000 w^******w^ 60 75 ............. TlZz~> 10 20 30 40 50 60 70 80 90 100 110 3.20 3.40 3.60 3.80

6406.D SCANAPR0902.M Thu May 02 14:10:00 2002 Page 4

NYC-WTC_000060280