GCMS Method 508 analysis results for April 9 2002

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Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\020409\0318LB.D Vial: 3 Acq On 9 Apr 2002 5:02 pm Operator: McLean Sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C: \MSDCHEM\1. . . \SC7\NAPR0902 .M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 1 1-Propyne, 3-chloro- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 3.30 0.25 ug/1 177047 1,4-Dichlorobenzene-d4 10.67 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Propyne, 3-chloro- 74 C3H3C1 000624-65-7 5 2 Propanoic acid 74 C3H6O2 000079-09-4 4 3 3-Buten-2-ol, 2-methyl- 86 C5H10O 000115-18-4 4 4 Azetidine, 1-methyl-______________ 71 C4H9N 004923-79-9 3 Abundance Scan 37 (3.296 min): 0318LB.D (-33) (-) m/z 43.10 100.00% 40 74 71 5000 40

I'''' I'''' I'''' I'''' I 47 3.20 3.30 3.40 3.50 3.60 3.70 86 m/z 74.00 75750% tVz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #108401:1 -Propyne, 3-chloro- 3)9

5000 74 3.20 3.30 3 40 3.50 3.60 3.70 in/z 71710 65730% 3f 43 47 51 57 p '' 11''' > 11' I ' ' I Ij . I rl I I . . I I I . . Tife-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 *\bundance #115: Propanoic acid 20 74 1 45 3.20 3 30 3.40 3 50 3.60 3.70 5000 m/z 47700 47783% 57 18 . . I.. ,iii.irr...,..ri;ini|iirTT.-;.,|ll,^„rv.. Il|,.. Tlfe-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #114555: 3-Bu1en-2-ol, 2-methyl- 43 I* 3.20 3.30 3.40 3.50 3.60 3.70 m/z477056780% 5000 59 31 39 1518 53 Tn-'-'l"l'l P)iiL|,,il|li 67, n/z-> 5 ..... I *1.wi. 86 -T+t^ 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 3.20 3.30 3.40 3.50 3.60 3.70

0318LB.D SCANAPR0902.M Thu May 02 14:02:30 2002 . Page 3

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