GCMS analysis results for sample AE05898, March 29 2002

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\MAR21O2\5898.D Vial: 26 Acq On : 22 Mar 2002 1:56 pm Operator: Sample : gc/ms scan 3/13 fb Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 ' Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 12.269 781 787 804 rBV 2211368 5007226 67.84% 12.962% 2 15.905 1177 1183 1200 rBV 3079540 6658983 90.22% 17.237% 3 21.220 1755 1762 1786 rBV 3384713 7380601 100.00% 19.105% 4 25.673 2239 2247 2257 rBV 3256145 7317562 99.15% 18.942% 5 25.801 2257 2261 2274 rVB 34453 89942 1.22% 0.233%

6 28.160 2512 2518 2533 rBV 1468050 2881161 39.04% 7.458% 7 30.428 2760 2765 2776 rVB 61983 112715 1.53% 0.292% 8 30.731 2793 2798 2804 rBV 218075 447216 6.06% 1.158% 9 33.733 3116 3125 3142 rBV2 2160500 5184290 70.24% 13.420% 10 33.935 3142 3147 3157 rVB 54968 126634 1.72% 0.328%

11 37.983 3578 3588 3602 rBV2 1064202 ■ 3424974 46.41% 8.866%

Sum of corrected areas: 38631304

5898.D GCMS0308.M Mon Mar 25 14:28:15 2002

NYC-WTC_000059772