NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed).
Data File C:\HPCHEM\1\DATA\APRO 402\5850.D Vial: 24
Acq On 4 Apr 2002 8:46 pm Operator:
Sample gc/ms scan 3/12 Inst : GC/MS 209
Mise Multiplr: 2.00
MS Integration Params: GOOFY.P
Quant Time: Apr 9 15:41 2002 Quant Results File: GCMS0408.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0408.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Last Update : Mon Apr 08 11:30:53 2002
Response via : Initial Calibration
DataAcq Meth : GCMS0403
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 12.24 152 353374 20.00 ug/1 -0.02 .
10) Naphthalene-d8 15.88 136 1281391 20.00 ug/1 -0.03
17) Acenaphthene-dlO 21.19 164 726682 20.00 ug/1 -o;o2
30) Phenanthrene-dlO 25.63 188 995309 20.00 ug/1 -0.03
39) Chrysene-dl2 33.69 240 477275 20.00 ug/1 -0.03
45) Perylene-dl2 37.93 264 262436 20.00 ug/1 -0.02
System Monitoring Compounds
2 8) TCMX 0.00 209 0 0.00 ug/mL
Spiked Amount 4.000 Recovery = 0.00%
. 38) 2,4-DDD 30.71 235 75820 -7.91 -ug/mL 0.21
Spiked Amount 5.000 Recovery
Target Compounds Qvalue
2) N-nitroso-dimethyl amine 5.47 74 257 N.D.
3) bis(2-Chloroethyl)ether 0.00 93 0 N.D.
4) 1,3-Dichlorobenzene 0.00 146 0 N.D.
5) 1,4-Dichlorobenzene 0.00 146 0 N.D.
6) 1,2-Dichlorobenzene 0.00 146 0 ■■
N.D.
7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D.
8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D.
9) Hexachloroethane 0.00 117 0 N.D.
11) Nitrobenzene 0.00 77 0 N.D.
12) Isophorone o.do 82 0 N.D.
13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D.
14) 1,2,4-Trichlorobenzene 0.00 180 0 ■ N.D.
15) Naphthalene 15.94 128 378 N.D.
16) Hexachlorobutadiene 0.00 225 0 N.D.
18) Hexachlorocyclopentadiene 0.00 237 0 N.D.
19) 2-Chloronaphthalene 0.00 162 0 N.D.
20) Dimethylphthalate 0.00 163 0 N.D.
21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d
2 2) Acenaphthylene 0.00 152 0 N.D.
23) Acenaphthene 0.00 153 0 N.D.
24) 2,4-Dinitrotoluene 0.00 165 0 N.D.
25) Diethylphthalate 22.67 149 949 N.D.
26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D.
27) Fluorene 0.00 166 0 N.D.
29) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
31) N-Nitrosodiphenylamine 0.00 168 0 N.D.
32) 4-Bromophenyl-phenylether 0.00 248 0 N.D.
(#) = qualifier out of range (m) = manual integration
5850.D GCMS0408.M Tue Apr 16 08:07:03 2002 Page 1
NYC-WTC_000059641
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