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GCMS reference data for sample AE05847, April 16 2002

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Reference data report listing component names and response values for calibration verification conducted on April 16, 2002.

NYC-WTC_000059608–000059618

Folder label: “GCMS X 3/12/02 A 4/4/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\APRO 402\5847.D Vial: 21 Acq On 4 Apr 2002 5:48 pm Operator: Sample- gc/ms scan 3/12 Inst : GC/MS 209 Mise Multiplr: 2.00 MS Integration Params: GOOFY.P Quant Time: Apr 9 15:37 2002 Quant Results File: GCMS0408.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0408.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon Apr 08 11:30:53 2002 Response via : Initial Calibration DataAcq Meth : GCMS0403

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 12.25 152 341726 20.00 ug/1 -0.01 10) Naphthalene-d8 15.89 136 1240285 20.00 ug/1 -0.02 17) Acenaphthene-dlO 21.18 164 706911 20.00 ug/1 -0.02 30) Phenanthrene-dlO 25.63 188 974550 20.00 ug/1 -0.03 . 39) Chrysene-dl2 33.69 240 462091 20.00 ug/1 -0.03 45) Perylene-dl2 37.93 264 251846 20.00 ug/1 -0.02 System Monitoring Compounds 2 8) TCMX 0.00 209 0 0.00 ug/mL Spiked Amount 4.000 Recovery = 0.00% 38) 2,4-DDD 30.71 235 ’«7-p5X' ug/mL 0.21 Spiked Amount 5.000 Recovery^.'7=^ Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0- N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 ■ 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.94 128 280 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.67 149 654 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 29) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 0.00 168 0 N.D. 32) 4-Bromophenyl-phenylether 0.00 248 0 N.D. (#) = qualifier out of range (m) = manual integration 5847.D GCMS0408.M Tue Apr 16 08:05:46 2002 Page 1

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