Laboratory method sheet for liquid-liquid extraction parameters

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Library Search Compound Report

Data File C:\HPCHEM\1\DATA\APRO 302\LBA.D Vial: 15 Acq On 4 Apr 2002 8:27 am Operator: Sample gc/ms scan 3/12 Inst : GC/MS 209 Mise Multiplr: 2.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0408.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Silane, tetramethyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. 8.13 4.06 ug/1 264869 1,4-Dichlorobenzene-d4 12.25 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Silane etramethyl- 88 C4H12Si 000075-76-3 47 2 N-Ethylfiormamide 73 C3H7NO 000627-45-2 9 3 1,3-Dioxolane, 2-pentadecyl- 284 C18H36O2 004360-57-0 9 4 3-Pentanol, 3-methyl-__________ _ 102 C6H14O 000077-74-7 9 Abundance / Scan 336 (8.129 min): LBA.D {-) m7z 73700 100.00% 73

5000 / 43 780 8.00 8.20 8.40 ,11 57 ,1 87 103 m/z 43.05 29.03% Tj-T-r-r-i-pH-i-VYTT^ ' ' 1 ' ' I'''' I' ''' I Tn/2-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #845: Silane, tetramethyl- 7(3

............ .. 5000 7.80 8.00 8.20 8;40 m/z 417705 10.21% 45 3? J 59 88................................... TiZz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #292: N-Ethylformamide -3 3

73 )............ 7.80 8.00 8.20 8.40 5000 m/z 44.95 9.77% 44 58

Tl/Z-> xJ, ' ' I ' ' 20 ill T-fTl 40 60 80 I'''' I'' ’ ‘ I I'''' I' ‘' I 100 120 140 160 180 200 220 240 260 280 Abundance #40191:1.3-Dioxolane, 2-pentadecyl- ___________ 70 7.80 8.00 8.20 8.40 m/z 71.00 67771% 5000

Tl/Z-> 20 4,3 57 40 60 80 86 99 256 283 100 120 140 160 180 200 220 240 260 280 | 7.80 8 00 K-r- 8,20 840

LBA.D GCMS0408.M Tue Apr 16 08:15:34 2002 Page 1

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