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GCMS analysis results for sample AE05743, April 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of sample AE05743 conducted on April 11, 2002, including surrogate recovery data.

NYC-WTC_000059536–000059544

Folder label: “GCMS X 3/12/02 A 4/2/02

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Scanned page image, NYC-WTC_000059543
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\APR0102\5744.D Vial: 23 Acq On 2 Apr 2002 11:00 pm Operator: Sample gc/ms scan 3/12 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 N-Ethylformamide Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.13 1.73 ug/1 260866 1,4-Dichlorobenzene-d4 12.25

Hit# of 5 Tentative ID MW MolForm ' CAS# Qual

1 N-Ethyl^ormamide 73 C3H7NO 000627-45-2 9 2 Silan^ tetramethyl- 88 C4H12Si 000075-76-3 9 3 1,3- ioxolane, 2-(3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 9 4 3-Pe tanol, 3-methyl- 102 C6H14O 000077-74-7 9 Abundance Scan 336 (^133 min^ (-) .. tn/T’.. 737^.... 100.00% 7b

5000 43 87 7.80 8.00 8.20 8.40 ........................... 3,7,1,1,49 55, 67, I 103 m/z 43.05 26.87% 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #292: N-Ethylformamide

5000 3|0

44 58 73

7.80 m/ z 8.00 J bv 8.20 8.40___ 10.48% 15 •I m/z-> 10 20 30 40____50 60 70 80 90 100 110 120 Abundance #52932. Silane, tetramcjfhvl- i 73 J.. ' 7.8o" ' 8.00 8.20 8.40 5000 m/z 45.05 10.28%

i 45 I 15 , , 53 59 I ' ' ' ' I ' ' ‘ ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' , , , , ,88......... ,,,,,,............. 'm/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #49423: 1,3-Dioxolane. 2-(3-bromo-5,5,Wrichloro-2,2-dimet 7i3 7.80 8.00 8.20__ 8.40 m/ z 71.00 6.89% A 5000 45 ......................... 36 II 55 ^■^1 ................ 1.09115 ' I ' ' ' ‘ I ' ' ' ' I ' ' * ' I ' ' ' '-'■■I-------- 1 ' ........ in/z-> 10 20 30 40 50 60 70 80 90 100 110 120 7.80 8.00 8.20 8.40

5744.D GCMS0403.M Fri Apr 05 10:37:01 2002 Page 1

NYC-WTC_000059543

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NYC-WTC_000059543Source: NYC Law Department, mirrored locally

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