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GCMS blank analysis results, sample AE05231, April 2002

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Laboratory report showing non-detect levels for various organic compounds in a GCMS blank sample from April 2002.

NYC-WTC_000059105–000059113

Folder label: “GCMS X 3/9/02 A 3/30/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\MAR3002\LBC.D Vial: 39 Acq On : 31 Mar 2002 6:39 am Operator: Sample : gc/ms scan 3/9 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 31 7:28 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 29 10:31:28 2002 Response via : Initial Calibration DataAcq Meth ': GCMS0308

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.25 152 417714 20.00 ug/1 -0.10 10) Naphthalene-d8 15.89 136 1515128 20.00 ug/1 -0.11 17) Acenaphthene-dlO 21.19 164 860319 20.00 ug/1 -0.12 29) Phenanthrene-dlO 25.63 188 1186088 20.00 ug/1 -0.14 38) Chrysene-dl2 33.69 240 562603 20.00 ug/1 -0.16 44) Perylene-dl2 37.93 264 314928 20.00 ug/1 -0.19

System Monitoring Compounds 37) 2,4-DDD 30.70 235 72898 6.13 ug/mL 0.21 Spiked Amount 5.000 Recovery = 122.60%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 12.15 146 290 N.D. 5) 1,4-Dichlorobenzene 12.30 146 317 N.D. 6) 1,2-Dichlorobenzene 12.82 146 258 N.D, 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 15.77 180 259 N.D. 15) Naphthalene 15.94 128 597 N.D. 16) Hexachlorobutadiene 16.48 225 377 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 2 3) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 0.00 149 0 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration LBC.D GCMS0308.M Wed Apr 03 13:33:40 2002 Page 1

NYC-WTC_000059106

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NYC-WTC_000059106Source: NYC Law Department, mirrored locally

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