NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\l\DATA\MAR2802\LBA.D Vial: 15
Acq On : 28 Mar 2002 10:26 pm Operator:
Sample : gc/ms scan 3/5 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: GOOFY.P
Quant Time: Apr 1 14:52 2002 Quant Results File: GCMS0308.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator)
Title ': 209 625/TCLP calibration table
Last Update : Fri Mar 29 10:31:28 2002
Response via : Initial Calibration
DataAcq Meth : GCMS0308
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 12.25 152 399139 20.00 ug/1 -0.10
10) Naphthalene-d8 15.88 136 1441692 20.00 ug/1 -0.12
17) Acenaphthene-dlO 21.19 164 820270 20.00 ug/1 -0.13
29) Phenanthrene-dlO 25.63 188 1157954 20.00 ug/1 -0.14
38) Chrysene-dl2 33.69 240 584184 20.00 ug/1 -0.15
44) Perylene-dl2 37.93 264 331674 20.00 ug/1 -0.19
System Monitoring Compounds ^/.4/
37) 2,4-DDD 30.71 235 85156 7-r3^ ug/mL 0.21
Spiked Amount 5.000 Recovery
Target Compounds Qvalue
2) N-nitroso-dimethyl amine 0.00 74 0 N.D.
3) bis(2-Chloroethyl)ether 0.00 93 0 N.D.
4) 1,3-Dichlorobenzene 12.15 146 256 N.D.
5) 1,4-Dichlorobenzene 12.29 146 354 N.D.
6) 1,2-Dichlorobenzene 12.81 146 256 N.D.
7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D.
8) N-Nitrosb-di-n-propylamine 0.00 70 0 N.D.
9) Hexachloroethane 0.00 117 0 N.D.
11) Nitrobenzene 0.00 77 0 N.D.
12) Isophorone 0.00 82 0 N.D.
13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D.
14) 1,2,4-Trichlorobenzene 15.78 180 190 N.D.
15) Naphthalene 15.94 128 635 N.D.
16) Hexachlorobutadiene 16.49 225 353 N.D.
18) Hexachlorocyclopentadiene 0.00 .237 0 N.D.
19) 2-Chloronaphthalene 0.00 162 0 N.D.
2 0) D.imethylphthalate 0.00 163 0 N.D.
■21) 2,6-Dinitrotoluene 0.00 165 0 N.D.
22) Acenaphthylene 0.00 152 0 N.D.
23) Acenaphthene 0.00 153 0 N.D.
24) 2,4-Dinitrotoluene 0.00 165 0 N.D.
25) Diethylphthalate 22.67 149 458 N.D.
26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D.
27) Fluorene 0.00 166 0 N.D.
28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration
LBA.D GCMS0308.M Mon Apr 01 14:53:39 2002 Page 1
NYC-WTC_000058488
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