Instrument calibration record using DFTPP standard to verify GCMS performance for analytical testing on April 1, 2002.
NYC-WTC_000059478–000059486Folder label: “GCMS X 3/12/02 A 4/2/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File C:\HPCHEM\l\DATA\APR0102\LBA.D Vial: 16 Acq On 2 Apr 2002 3:07 am Operator : Sample gc/ms scan 3/12 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 5 9:37 2002 Quant Results File: GCMS0308.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 29 10:31:28 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 12.25 152 531703 20.00 ug/1 -0.11 10) Naphthalene-d8 15.88 136 1943158 20.00 ug/1 -0.12 17) Acenaphthene-dlO 21.19 164 1101902 20.00 ug/1 -0.12 29) Phenanthrene-dlO 25.63 188 1591273m 20.00 ug/1 -0.13 38) Chrysene-dl2 33.69 240 786020 20.00 ug/1 -0.15 44) Perylene-dl2 37.93 264 426319 20.00 ug/1 -0.19
System Monitoring Compounds 37) 2,4-DDD 30.71 235 74939 4.69 ug/mL 0.21 Spiked Amount 5.000 Recovery = 93.80%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene ,0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.94 128 193 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D-. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.67 149 1059 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration LBA.D GCMS0403.M Fri Apr 05 09:38:09 2002 Page 1
NYC-WTC_000059479
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NYC-WTC_000059589
Technical record detailing laboratory method parameters including drip rates and reagent volumes for sample processing.
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Laboratory report showing GCMS blank analysis for volatile organic compounds on March 29, 2002.
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Laboratory report showing GCMS blank analysis results for sample AE01156 conducted on March 25, 2002, with compound detection limits.
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Laboratory report showing non-detect levels for various organic compounds in a GCMS blank sample from April 2002.
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Laboratory report showing non-detect levels for various organic compounds in a GCMS blank sample from April 2002.
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Quality control blank analysis results for GC/MS testing of sample AE04038 conducted on March 27, 2002.
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Laboratory report documenting a blank sample analysis for GCMS testing of volatile organic compounds in April 2002.
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Laboratory report showing GCMS blank analysis for sample AE09095 conducted on April 23, 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047643
Laboratory report of a GCMS blank analysis for sample AE08012 conducted on April 17, 2002, showing non-detect levels for various compounds.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000014611
Laboratory report showing GCMS blank analysis results for volatile organic compounds in sample AE12535 on June 3-4, 2002.
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Laboratory report showing blank analysis results for volatile organic compounds in sample AE05750 from April 2002.
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Laboratory data sheet recording GCMS blank analysis parameters for sample AE09579 conducted on May 8, 2002.
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NYC-WTC_000059487
Laboratory report of a GCMS blank test conducted on April 5, 2002, showing non-detect levels for various organic compounds.
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Calibration data sheet listing retention times and response factors for multiple organic compounds analyzed on April 5, 2002.
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