NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\l\DATA\MAR3002\LBB.D Vial: 26
Acq On : 30 Mar 2002 5:45 pm Operator:
Sample : gc/ms scan 3/8 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: GOOFY.P
Quant Time: Mar 30 18:34 2002 Quant Results File: GCMS0308.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Last Update : Fri Mar 29 10:31:28 2002
Response via : Initial Calibration
DataAcq Meth : GCMS0308
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 12.25 152 439495 20.00 ug/1 -0.10
10) Naphthalene-d8 15.88 136 1627500 20.00 ug/1 -0.11
17) Acenaphthene-dlO 21.19 164 911636 20.00 ug/1 -0.12
29) Phenanthrene-dlO 25.63 188 1268917 20.00 ug/1 -0.13
' 38) Chrysene-dl2 33.69 240 616628 20.00 ug/1 -0.15
44) Perylene-dl2 37.94 264 349277 20.00 ug/1 -0.19
System Monitoring Compounds
37) 2,4-DDD 30.71 235 / 83214/ ug/mL
Spiked Amount 5.000 Recovery
Target Compounds Qvalue
2) N-nitroso-dimethyl amine 5.55 74 100 N.D.
3) bis(2-Chloroethyl)ether 11.51 93 181 N.D.
4) 1,3-Dichlorobenzene 12.15 146 836 N.D.
5) 1,4-Dichlorobenzene 12.30 146 771 N.D.
6) 1,2-Dichlorobenzene 12.81 146 521 N.D.
7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D.
8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D.
9) Hexachloroethane 13.66 117 224 N.D.
11) Nitrobenzene 0.00 77 0 N.D.
12) Isophorone 0.00 82 0 N.D.
13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D.
14) 1,2,4-Trichlorobenzene 15.77 180 556 N.D.
15) Naphthalene 15.94 128 763 N.D.
16) Hexachlorobutadiene 16.49 225 536 N.D.
18) Hexachlorocyclopentadiene 0.00 237 0 N.D.
19) 2-Chloronaphthalene 19.47 162 202 N.D.
20) Dimethylphthalate 0.00 163 0 N.D.
21) 2,6-Dinitrotoluene 0.00 165 0 N.D.
22) Acenaphthylene 0.00 152 0 N.D.
23) Acenaphthene 0.00 153 0 N.D.
24) 2,4-Dinitrotoluene 0.00 165 0 N.D.
25) Diethylphthalate 22.68 149 523 N.D.
26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D.
27) Fluorene 0.00 166 0 N.D.
28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration
LBB.D GCMS0308.M Tue Apr 02 15:10:08 2002 Page 1
NYC-WTC_000058899
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