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GCMS sample AE05055 analysis, April 2002

Machine-extracted title · confidence 100%

Laboratory report for sample AE05055 analyzing unknown compounds and surrogates via GCMS on April 9, 2002.

NYC-WTC_000058929–000058937

Folder label: “GCMS X 3/8/02 A 3/30/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\l\DATA\MAR3002\5054.D Vial: 30 Acq On : 30 Mar 2002 9:43 pm Operator: Sample : gc/ms scan 3/8 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.136 333 337 346 rBV 42073 101020 2.62% 0.585% 2 12.249 780 785 801 rVB 1117448 2642078 68.47% 15.312% 3 15.884 1175 1181 1198 rBV 1671840 3404166 88.22% 19.729% 4 21.191 1753 1759 1771 rBV 1918164 3858570 100.00% 22.362% 5 25.634 2236 2243 2253 rBV2 1703373 3538688 91.71% 20.509%

6 30.711 2791 2796 2803 rVB 236496 455568 11.81% 2.640% 7 33.694 3114 3121 3139 rBV 881135 1979916 51.31% 11.475% 8 37.935 3575 3583 3603 rBV2 421481 1274644 33.03% 7.387%

Sum of corrected areas: 17254650

5054.D GCMS0308.M Tue Apr 02 15:32:26 2002

NYC-WTC_000058934

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NYC-WTC_000058934Source: NYC Law Department, mirrored locally

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