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GCMS calibration table data, March 2002

Machine-extracted title · confidence 100%

Calibration table and chromatogram data for sample AE04942 from March 29, 2002.

NYC-WTC_000058663–000058667

Folder label: “GCMS X 3/6/02 A 3/30/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\l\DATA\MAR3002\4942.D Vial: 9 Acq On : 29 Mar 2002 10:53 pm Operator: Sample : gc/ms scan 3/6 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 12.254 779 785 798 rVB 958636 2450152 68.73% 15.153% 2 14.843 1062 1067 1072 rBV 34786 69208 1.94% 0.428% 3 15.880 1174 1180 1198 rBV 1442634 3137665 88.01% 19.405% 4 21.186 1752 1758 1778 rBV 1642037 3564979 100.00% 22.047% 5 25.630 2236 2242 2254 rBV2 1512155 3303973 92.68% 20.433%

6 30.706 2790 2795 2801 rBV 191699 372436 10.45% 2.303% 7 33.690 3113 3120 3141 rBV2 842554 1943860 54.53% 12.022% 8 37.931 3574 3582 3604 rBV2 430045 1327336 37.23% 8.209%

Sum of corrected areas: 16169609

4942.D GCMS0308.M Tue Apr 02 11:05:58 2002

NYC-WTC_000058664

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NYC-WTC_000058664Source: NYC Law Department, mirrored locally

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