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GCMS surrogate recovery data for sample AE04945, April 2002

Machine-extracted title · confidence 100%

Record of surrogate compound recovery rates for sample AE07634 analyzed on April 30, 2002.

NYC-WTC_000040212–000040229

Folder label: “GCMS X 4/3/02 A 4/10/02

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Scanned page image, NYC-WTC_000040226
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document LSC Area Percent Report

Data File : C:\HPCHEM\l\DATA\MAR3002\4945.D Vial: 12 Acq On : 30 Mar 2002 1:52 am Operator: Sample : gc/ms scan 3/6 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 12.245 779 784 798 rBV 990645 2459692 68.75% 15.460% 2 14.843 1061 1067 1073 rBV 67610 133465 3.73% 0.839% 3 15.881 1174 1180 1198 rBV 1492796 3163906 88.43% 19.886% 4 21.187 1752 1758 1771 rBV 1712604 3577737 100.00% 22.487% 5 25.630 2235 2242 2254 rBV2 1525861 3292049 92.01% 20.692%

6 30.707 2790 2795 2802 rVB 189654 365252 10.21% 2.296% 7 33.690 3109 3120 3126 rBV2 833413 1785862 49.92% 11.225% 8 37.932 3575 3582 3597 rBV2 378494 1132051 31.64% 7.115%

Sum of corrected areas: 15910014

4945.D GCMS0308.M Tue Apr 02 11:07:59 2002

NYC-WTC_000040226

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NYC-WTC_000040226Source: NYC Law Department, mirrored locally

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