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GCMS analysis report, sample AE04450, April 2002

Machine-extracted title · confidence 100%

Gas chromatography-mass spectrometry results for sample AE04450 analyzed on April 4, 2002.

NYC-WTC_000012372–000012380

Folder label: “GCMS X 3-1-02 A 3-21-02

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Scanned page image, NYC-WTC_000012377
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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\l\DATA\MAR2102\4450.D Vial: 13 Acq On : 21 Mar 2002 11:07 pm Operator: Sample : gc/ms scan 3/1 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % Of # min scan scan scan TY height area % max. total

1 8.143 333 337 347 rBV 164462 362197 7.63% 1.552% 2 12.265 780 786 808 rVB 1452497 3258408 68.64% 13.965% 3 15.900 1176 1182 1199 rBV 2024214 4342592 91.48% 18.611% 4 21.216 1754 1761 1779 rBV 2325809 4747227 100.00% 20.346% 5 25.659 2238 2245 2256 rBV2 2126063 4687253 98.74% 20.088%

6 30.735 2792 2798 2803 rBV 188720 378522 7.97% 1.622% 7 33.719 3116 3123 3141 rBV2 1390952 3350451 70.58% 14.359% 8 37.979 3578 3587 3605 rBV2 719138 2206399 46.48% 9.456%

Sum of corrected areas: 23333049

4450.D GCMS0308.M Fri Mar 22 09:44:02 2002

NYC-WTC_000012377

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NYC-WTC_000012377Source: NYC Law Department, mirrored locally

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