GCMS analysis page for sample AE05050, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\MAR3OO2\5O5O.D Vial: 23 Acq On 30 Mar 2002 12:47 pm Operator: Sample gc/ms scan 3/7 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

^Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.23 0.52 ug/1 65994 ■ 1,4-Dichlorobenzene-d4 12.25

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pent^one, 4-hydroxy-4-methyl - 116 C6H12O2 000123-42-2 39 2 Oxira: [ (1-methylethoxy)methyl] - 116 C6H12O2 004016-14-2 38 3 Morp^line, 4-methyl- 101 C5H11NO 000109-02-4 9 4 Pro] 2-methoxy- 74 C4H10O 000598-53-8 9 Abundance' ........ Scan 34778)228 m/z 43.05 100.00% 4)3

59 5000-

101 AJ ,..4.3... ' 83 I 7.80 “m/z 8.00 59.05 8.20__ 8.40 50.65% 8.60 ______ 10____ 20____ 30 40 50 60 70 80 90 100 110 Abundance #64275; 2-Pentanone, 4-hydroxy-4-methyi- 413

5000 59 7.80 8.00 8.20 8.40 8.60 •; 15 m/z 100.95 20.15% 31 101 T-r-r-r-lr m/2-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #3238; Oxirane. [(1 -inethylethoxyjtneihyl]- 4'3 59 ............................................ 7.80 8.00 8.20 8.40 8.60 5000 m/ z 58.0 14.76% 31 73 101 ' I ' ' ' ' I m/z->W 20...... 30. 40 50 60 ' '7'0' s'o' 90 ' 160 ' ' 110 Abundance #1640: Morpholine, 4-methyl- 4i3 7.80 8.00 8.20 8.40 8.60 m/z 41.0,0 7.76% 5000 /I 15 101 27 71 I il .......... 56 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40 8.60 |

5050.D GCMS0308.M Tue Apr 02 14:11:20 2002 Page 1

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