GCMS analysis results for sample AE12574, June 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\JUN0302\12574.D Vial: .25 Acq On 4 Jun 2002 8:54 am Operator: Sample gc/ms scan 5/28 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 8.07 0.84 ug/1 57528 1,4-Dichlorobenzene-d4 12.07 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pent tone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 45 2 1,8-N< anediol, 8-methyl- 174 C10H22O21 054725-73-4 9 3 Oxir e, 3-ethyl-2,2-dimethyl- 100 C6H12O 001192-22-9 9 4 Ace mide 59 C2H5NO 000060-35-5 5 Abundance Scan 329 (8.066 min): 12574.D (-) m/z 42.90 100.00% 43

59 5000

101 ITTI14IITT 7.801 8.00 8.20 8.40 —P +49 + I ■ • ■ ■ i 1 ■ 1 83 i ''' ' ■ i ■ ■ ■ h ■ ■ ■ • i ■ • ■ • i ■ ■ ■ • i ' m/z !59.00। 53.69% miz-> 20 30 40 50 _________________ 60 70 80 90 100 110 120 130 Abundance #64274:2-Pentanone, 4-hydroxy-4-methyl- 43

5000 59 7.80 8.00 8.20 8.40 m/z 58.00 21.21% 27 I 0 101 ..... __

n/z-> I, . 20 30 40 +4950— ----- 60 70 80 90 100 110 120 130 Abundance #46264:1,8-Nonanediol, 8-methyl- 59 s MAA.A ...... 7.80 8.00 8.20 8.40 5000 m/z 100.95 19.25%

42 11999— l„ , 69, 83 98 123 iz-> 20 30 40 50 I60 70 80 90 100 110 120 130 Abundance #63346: Oxirane, 3-ethyl-2,2-dimethyl- 59 7.80 8.00 8.20 8.40 41 m/z 41.00 7.39%

5000

85

m/z—> •1t*"41‘*45 I " ' i 20 30 40 50 53 60 m 70 80 71 ‘ 1 • i ■ 90 1 ' i ■ ■ 1 1 l 1 ' ' 1 I 1 100 110 120 — AA_AAA 130 7.80 8.00 8.20 8.40

12574.D GCMS0531.M Tue Jun 04 11:53:26 2002 Page 1

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