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← Document results/DEP Box 57/GCMS X 3/7/02 A 3/27/02
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GCMS analysis page, sample AE05032, March 2002

Machine-extracted title · confidence 100%

Laboratory report page showing surrogate recovery data for sample AE05032 analyzed on March 29, 2002.

NYC-WTC_000058771–000058779

Folder label: “GCMS X 3/7/02 A 3/27/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR2602\5032.D Vial: 24 Acq On : 27 Mar 2002 8:32 am Operator: Sample : gc/ms scan 3/7 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Cyclopentasiloxane, decamethyl Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

14.84 0.61 ug/1 147845 Naphthalene-d8 15.89

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopent iloxane, decamethyl- 370 C10H3005Si5 000541-02-6 59 2 3,4-Dihyd oxybenzyl alcohol,tris(tr 356 C16H32O3Si3 068595-79-9 53 3 Pheneth^i^amine, N-methyl- . beta . , 3,4 399 C18H37NO3Si3 010538-85-9 38 4 N-(Trifiuoroacetyl)-N,0,O',C ' O''-tetr 553 C22H42F3NO4Si4 000000-00-0 32 Abundance Scan 1067 (14.M4 min): 5032.D (-) .... .................... ...... m/z.... 737m.. .. Yqo;oo%! 73

5000 267 355

I ‘ ' 45 108 125 I 1M J 77 93 223 251 14.60 14.80 15.00 15.20 Vpt 323 339 L m/z 267.00 41.88% m/Z;-> 40 60 .. 80 ,100.. 120 140 160 180 200_, 220_ 24.0 26Q 280 300 320 340 360 Abundance #51266: Cyclopentasiloxsne, decamethyi- 73

5000 267 355 n . _____ 14.60 14.80 15.00 15.20 m/z 355.05 39.40% i 191 207 251 , p-r-rp-m- Wz->40 60 80 100 120 140 160 180 200 220 240 260 280 300 320340 360 Abundance #49358: .j.J-t^bydroxyber'zy' s'cciici ttisilrrmethylsilyi)- 73 I 14.60 14.80 15.00 15.20 267 5000 179 m/z 356.05 15.48% 356 45 147 209 237 312 341 , -n-p-rr-p-r n -p-n-rp-TT-rj-T

n rT-T-rymT-r-qT-T-T-ry m/z->40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #74239: Phenethyiamine, N-methyl-.beta.,3,4-tris(trimethyis 3 14.60 14.80 15.00 15.20 m/ z 2 68.00 12.17% 5000 355 44 , 88 130 147 193 267 294 I, n-' >" I -p-r-TTy-rt-T- ' " I'''' I'''' I p m/z--> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 14.60 14.80 15.00 15.20

5032.D GCMS0308.M Fri Mar 29 11:37:03 2002 Page 1

NYC-WTC_000058778

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NYC-WTC_000058778Source: NYC Law Department, mirrored locally

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