GCMS analysis results, sample AE04947, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\MAR3 OO2\4947.D Vial: 14 Acq On : 30 Mar 2002 3:51 am Operator: Sample : gc/ms scan 3/6 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 1,1,1,5,7,7,7-Heptamethyl-3,3- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

38.83 1.29 ug/1 86189 Perylene-dl2 37.94

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 25 2 3,6-Dioxa-2,4,/5,7-tetrasilaoctane, 294 C10H3002Si4 004342-25-0 17 3 N-Methyl-m-hei#ipimide 221 C11H11N04 000000-00-0 10 .1 ' 3_(2H,4H) -Isfoquinolinedione, 6,7-d 369 C20H19NO6 000000-00-0 10 Abundance 73 Scan 3680 (38.826 min): 4947.D (-) m/z... 73;00 iooTo^ 147 221 5000 281 355 429

m/z-> 49 -p-ATyTrXy I 193

40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 I 327 lL X4, 3MO J8.6O J8.8O J9^O^39JO

Abundance #56714; 1,'l,1,5,7,7,7-Heptamefhyl-3,3-bis(trimethylsiioxy)t Tp 147 5000 267 355 429 38:40_J8J0_38^J9.p0_^9^0__ 45 207 m/z 221.0,5 57.15% i I I I m/Zj^___ 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 Abundance #41682: 3.6-Dio?;a-2.4,57-ictrasilaorane, 2.2.4.4,5.5.7.7- 147 221

73 38.40 38.60 38.80 39.00 39.20 5000 m/z 355.05 34.60% 191 117 279 .........,, ,,,,1............................................................ rnfe”>____ 40 60 80 100120140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 Abundance 'ii277QQ: N-Memyl-ni-hemipimide " ......... 22l 38.40 38.60 38.80 39.00 39.20 m/z 281.LO 30.58% 5000

50 93 T M ,, , I „ I I „ J.................................. .... 33^ 40 60 80 100 120 140 160180 200 220 240 260 280 300 320 340 360 380 400 420 38.40 38.60 38.80 39.00 39.20

4947.D GCMS0308.M Tue Apr 02 11:10:31 2002 Page 4

NYC-WTC_000058707