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GCMS analysis results for sample AE04846, April 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE04846 conducted on April 5, 2002.

NYC-WTC_000058571–000058579

Folder label: “GCMS X 3/5/02 A 3/29/02

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Scanned page image, NYC-WTC_000058576
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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\l\DATA\APR0102\4846.D Vial: 29 Acq On 1 Apr 2002 5:11 pm Operator: Sample gc/ms scan 3/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 12.245 779 784 799 rVB 1086200 2576721 68.38% 15.118% 2 15.890 1175 1181 1195 rBV 1540773 3303834 87.68% 19.384% 3 21.196 1752 1759 1778 rBV 1739447 3768041 100.00% 22.107% 4 25.640 2236 2243 2254 rBV2 1632492 3542540 94.02% 20.784% 5 25.777 2254 2258 2269 rVB2 14295 39642 1.05% 0.233%

6 30.707 2790 2795 2801 rBV 263669 529712 14.06% 3.108% 7 33.691 3114 3120 3136 rBV2 878149 1999548 53.07% 11.731% 8 37.941 3575 3583 3601 rBV2 432514 1284412 34.09% 7.536%

Sum of corrected areas: 17044450

4846.D GCMS0308.M Tue Apr 02 08:16:34 2002

NYC-WTC_000058576

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NYC-WTC_000058576Source: NYC Law Department, mirrored locally

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