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GCMS chromatogram data for sample AE04594, April 2002

Machine-extracted title · confidence 100%

Analytical run record from April 2, 2002, documenting unknown compounds and surrogate recovery for sample AE04594.

NYC-WTC_000058416–000058425

Folder label: “GCMS X 3/4/02 A 3/26/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\MAR2602\4594.D Vial: 10 Acq On : 26 Mar 2002 6:37 pm Operator: Sample : gc/ms scan 3/4 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 26 19:26 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Mar 26 14:13:06 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorohenzene 0.00 284 0 N.D. 33) Phenanthrene 25.64 178 436 N.D. 34) Anthracene 25.70 178 140 N.D. 35) Di-n-butylphthalate 27.60 149 3073 N.D. 36) Fluoranthene 0.00 202 0 N.D. 39) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo(a)anthracene 33.69 228 1844 N.D. 42) Bis(2-ethylhexyl)phthalate 33.91 149 1618 N.D. 43) Chrysene 33.69 228 1844 N.D. 45) Di-n-Octylphthalate 0.00 149 0 N.D. 46) Benzo(b)fluoranthene 36.81 252 196 N.D. 47) Benzo(k)fluoranthene 36.81 252 196 N.D. 48) Benzo(a)pyrene 37.95 252 1926 N.D. 49) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 4594.D GCMS0308.M Thu Mar 28 16:00:54 2002 Page 2

NYC-WTC_000058419

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NYC-WTC_000058419Source: NYC Law Department, mirrored locally

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