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GCMS analysis report, sample AE04336, March 25 2002

Machine-extracted title · confidence 85%

Gas chromatography-mass spectrometry analysis of sample AE04336 conducted on March 25, 2002, identifying other unknown compounds.

NYC-WTC_000038817–000038826

Folder label: “GCMS X 3/4/02 A 3/20/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\MAR1902\4336.D Vial: 29 Acq On : 21 Mar 2002 8:38 am Operator : Sample : gc/ms scan 3/4 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 21 14:10 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 08 08:54:27 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 25.65 178 590 N.D. 34) Anthracene 25.65 178 590 N.D. 35) Di-n-butylphthalate 27.63 149 3073 N.D. 36) Fluoranthene 0.00 202 0 N.D. 39) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo(a)anthracene 33.72 228 2153 N.D. 42) Bis(2-ethylhexyl)phthalate 33.92 149 904 N.D. 43) Chrysene 33.72 228 2154 N.D. 45) Di-n-Octylphthalate 0.00 149 0 N.D. 46) Benzo(b)fluoranthene 0.00 252 0 N.D. 47) Benzo(k)fluoranthene 0.00 252 0 N.D. 48) Benzo(a)pyrene 37.97 252 2592 N.D. 49) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 4336.D GCMS0308.M Thu Mar_ 21 14:11:56 2002 Page 2

NYC-WTC_000038820

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NYC-WTC_000038820Source: NYC Law Department, mirrored locally

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