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GCMS analysis results, sample AE04132, April 2002

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Gas chromatography-mass spectrometry analysis of environmental sample AE04132 conducted April 1, 2002, measuring organic compounds including 2,4-DDD surrogate.

NYC-WTC_000011779–000011788

Folder label: “GCMS X 2/25/02 A 3/23/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\MAR2202\4132.D Vial: 28 Acq On : 23 Mar 2002 10:42 pm Operator: Sample : gc/ms scan 2/25 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 27 9:56 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Mar 26 14:13:06 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 3 3) Phenanthrene 25.66 178 405 N.D. 3 4) Anthracene 25.66 178 405 N.D. 35) Di-n-butylphthalate 27.63 149 8143 N.D. 36) Fluoranthene 0.00 202 0 N.D. 3 9) Pyrene 0.00 202 0 N.D. 4 0) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo(a)anthracene 33.72 228 2097 N.D. 42) Bis(2-ethylhexyl)phthalate 33.93 149 13486 0.36 ug/1 # 88 43) Chrysene 33.72 228 2097 N.D. 45) Di-n-Octylphthalate 35.69 149 722 N.D. 46) Benzo(b)fluoranthene 0.00 252 0 N.D. 47) Benzo(k)fluoranthene 0.00 252 0 N.D. 4 8) Benzo(a)pyrene 37.98 252 2450 N.D. 4 9) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

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(#) = qualifier out of range (m) = manual integration 4132.D GCMS0308.M Wed Mar 27 09:58:02 2002 Page 2

NYC-WTC_000011782

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NYC-WTC_000011782Source: NYC Law Department, mirrored locally

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