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Laboratory blank results, sample AD28048, Dec 2001

Machine-extracted title · confidence 95%

Laboratory blank analysis results for sample AD28048 showing pesticide compound levels below detection limits on December 18, 2001.

NYC-WTC_000058107–000058109

Folder label: “525 X 11/26/01 A 12/14 - 12/15/01

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\MSDCHEM\1\DATA\1214 01\1214LB.D Vial: 12 Acq On : 15 Dec 2001 1:04 am Operator: McLean Sampl : 11/26/01 525 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: BENZO.P Quant Time: Dec 18 09:40:14 2001 Quant Results File: 121401.RES

Quant Method : C:\MSDCHEM\l\5973N\121401.M (RTE Integrator) Title : Quantitation For Method 525.2 Last Update : Tue Dec 18 09:35:41 2001 Response via : Initial Calibration DataAcq Meth : 120501

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) Acenaphthene-dlO 18.21 164 5265665 5.00 ug/L 0.00 9) Phenanthrene D-10 22.53 188 8134670 5.00 ug/L 0.00 20) Chrysene D-12 30.30 240 5244827 5.00 ug/L 0.00

System Monitoring Compounds 2) 1,3-Dimethyl-2-nitrobenzen 13.13 134 1369769 5.09 ug/L 0.00 Spiked Amount 5.000 Recovery = 101.80% 19) Triphenyl Phosphate surr 29.58 326 1168269 4.72 ug/L 0.00 Spiked Amount 5.000 Recovery = 94.40% 21) Perylene D-12 surr 34.31 264 3401416 4.91 ug/L 0.00 Spiked Amount 5.000 Recovery = 98.20%

Target Compounds Qvalue 3) Hexachlorocyclopentadiene 0.00 237 0 N.D. 4) Hexachlorobenzene 0.00 284 0 N.D. d 5) EPTC 0.00 128 0 N.D. 6) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 7) 2,4-Dinitotoluene 0.00 165 0 N.D. d 8) Molinate 0.00 126 0 N.D. d 10) Simazine 0.00 201 0 N.D. 11) Atrazine 0.00 200 0 N.D. 12) Alachlor 0.00 160 0 N.D. 13) Terbacil 0.00 161 0 N.D. d 14) Acetochlor 0.00 146 0 N.D. 15) Metribuzin 0.00 198 0 N.D. 16) Metdlachlor 0.00 162 0 N.D. 17) Butachlor 0.00 160 0 N.D. d 18) 4,4'-DDE 27.29 246 7965 0.03 ug/L 78 22) Bis (2-Ethylhexyl) adipate 29.51 129 12489 0.40 ug/L # 57 23) Bis (2-Ethylhexyl) phthala 30.96 149 150805 0.47 ug/L 97 24) Benzo (a) pyrene 0.00 252 0 N.D. d

(#) = qualifier out of range (m) = manual integration 1214LB.D 121401.M Tue Dec 18 09:41:09 2001 Page 1

NYC-WTC_000058108

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NYC-WTC_000058108Source: NYC Law Department, mirrored locally

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