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← Document results/DEP Box 30/525 X 11/28/01 A 12/19/01
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Method 525 pesticide results, sample AD28322, Dec 2001

Machine-extracted title · confidence 90%

Laboratory report for sample AD28322 showing non-detects for pesticides and contaminants analyzed on December 19, 2001.

NYC-WTC_000055825–000055827

Folder label: “525 X 11/28/01 A 12/19/01

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\MSDCHEM\1\DATA\121801\1128LB.D Vial: 49 Acq On : 18 Dec 2001 5:05 pm Operator: McLean Sample : 11/28 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: BENZO.P Quant Time: Dec 19 10:52:55 2001 Quant Results File: 121401.RES

Quant Method : C:\MSDCHEM\l\5973N\121401.M (RTE Integrator) Title : Quantitation For Method 525.2 Last Update : Tue Dec 18 09:35:41 2001 Response via : Initial Calibration DataAcq Meth : 121401

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) Acenaphthene-dlO 18.20 164 6871203 5.00 ug/L 0.00 9) Phenanthrene D-10 22.53 188 10838575 5.00 ug/L 0.00 20) Chrysene D-12 30.31 240 7341310 5.00 ug/L 0.00

System Monitoring Compounds 2) 1,3-Dimethyl-2-nitrobenzen 13.13 134 1561922 4.44 ug/L 0.00 Spiked Amount 5.000 Recovery = 88.80% 19) Triphenyl Phosphate surr 29.58 326 1738034 5.27 ug/L 0.00 Spiked Amount 5.000 Recovery = 105.40% 21) Perylene D-12 surr 34.32 264 4831305 4.98 ug/L 0.00 Spiked Amount 5.000 Recovery = 99.60%

Target Compounds Qvalue 3) Hexachlorocyclopentadiene 0.00 237 0 N.D. 4) Hexachlorobenzene 0.00 284 0 N.D. 5) EPTC 0.00 128 0 N.D. 6) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 7) 2,4-Dinitotoluene 18.95 165 2618 0.31 ug/L 80 8) Molinate 0.00 126 0 N.D. d 10) Simazine 0.00 201 0 N.D. 11) Atrazine 0.00 200 0 N.D. 12) Alachlor 0.00 160 0 N.D. 13) Terbacil 0.00 161 0 N.D. d 14) Acetochlor 0.00 146 0 N.D. 15) Metribuzin 0.00 198 0 N.D. 16) Metolachlor 0.00 162 0 N.D. 17) Butachlor 0.00 160 0 N.D. d 18) 4,4'-DDE 0.00 246 0 N.D. d 22) Bis (2-Ethylhexyl) adipate 29.58 129 26834 0.40 ug/L 79 23) Bis (2-Ethylhexyl) phthala 30.96 149 149613 0.45 ug/L 98 24) Benzo (a) pyrene 0.00 252 0 N.D. d

(#) = qualifier out of range (m) = manual integration 1128LB.D 121401.M Wed Dec 19 10:53:31 2001 Page 1

NYC-WTC_000055826

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NYC-WTC_000055826Source: NYC Law Department, mirrored locally

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