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Method 525 pesticide results, sample AD28324, Dec 2001

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Laboratory report for sample AD28324 showing non-detects for pesticides and contaminants analyzed on December 20, 2001.

NYC-WTC_000055786–000055788

Folder label: “525 X 11/27/01 A 12/17 - 12/18/01

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\MSDCHEM\1\DATA\121701\1127LBB.D Vial: 43 * Acq On : 18 Dec 2001 8:03 am Operator: McLean Sample : 11/27 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: BENZO.P Quant Time: Dec 18 08:40:22 2001 Quant Results File: 121401.RES

Quant Method : C:\MSDCHEM\l\5973N\121401.M (RTE Integrator) Title : Quantitation For Method 525.2 Last Update : Mon Dec 17 15:06:05 2001 Response via : Initial Calibration DataAcq Meth : 121401

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) Acenaphthene-diO 18.20 164 6782380 5.00 ug/L 0.00 9) Phenanthrene D-10 22.53 188 10470924 5.00 ug/L 0.00 20) Chrysene D-12 30.31 240 7399684 5.00 ug/L 0.00

System Monitoring Compounds 2) 1,3-Dimethyl-2-nitrobenzen 13.13 134 1594209 4.60 ug/L 0.00 Spiked Amount 5.000 Recovery = 92.00% 19) Triphenyl Phosphate surr 29.59 326 1682675 5.28 ug/L 0.00 Spiked Amount 5.000 Recovery = 105.60% 21) Perylene D-12 surr 34.32 264 5233721 5.35 ug/L 0.00 Spiked Amount 5.000 Recovery = 107.00%

Target Compounds Qvalue 3) Hexachlorocyclopentadiene 0.00 237 0 N.D. 4) Hexachlorobenzene 21.39 284 13801 0.03 ug/L 89 5) EPTC 0.00 128 0 N.D. 6) 2,6-Dinitrotoluene 17.82 165 8581 0.33 ug/L # 54 7) 2,4-Dinitotoluene 18.95 165 1620 0.31 ug/L # 21 8) Molinate 18.98 126 12945 0.01 ug/L # 1 10) Simazine 0.00 201 0 N.D. 11) Atrazine 0.00 200 0 N.D. 12) Alachlor 0.00 160 0 N.D. 13) Terbacil 0.00 161 0 N.D. d 14) Acetochlor 0.00 146 0 N.D. 15) Metribuzin 0.00 198 0 N.D. 16) Metolachlor 0.00 162 0 N.D. 17) Butachlor 0.00 160 0 N.D. d 18) 4,4'-DDE 0.00 246 0 N.D. d 22) Bis (2-Ethylhexyl) adipate 29.52 129 10927 0.39 ug/L # 10 23) Bis (2-Ethylhexyl) phthala 30.96 149 325916 0.52 ug/L 94 24) Benzo (a) pyrene 0.00 252 0 N.D. d

(#) = qualifier out of range (m) = manual integration 1127LBB.D 121401.M Thu Dec 20 10:57:34 2001 Page 1

NYC-WTC_000055787

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NYC-WTC_000055787Source: NYC Law Department, mirrored locally

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