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Calibration standard analysis results, sample AD27547, Nov-Dec 2001

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Laboratory report listing analytical results for pesticides and organic compounds in calibration standard AD27547.

NYC-WTC_000057724–000057726

Folder label: “525 11/15/01 12/6 - 12/7 12/4 - 12/5 TWO INSTR.

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\MSDCHEM\1\DATA\120501\1116LB.D Vial: 5 Acq On : 5 Dec 2001 6:24 pm Operator: McLean ample : 11/16 run ' Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: BENZO.P Quant Time: Dec 11 09:10:34 2001 Quant Results File: 120501.RES

Quant Method : C:\MSDCHEM\1\5973N\120501.M (RTE Integrator) Title : Quantitation For Method 525.2 Last Update : Thu Dec 06 10:31:04 2001 Response via : Initial Calibration DataAcq Meth : 120501

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) Acenaphthene-d10 18.31 164 4810429 5.00 ug/L 0.00 9) Phenanthrene D-10 22.64 188 7400763 5.00 ug/L 0.00 20) Chrysene D-12 30.42 240 5218776 5.00 ug/L 0.00

System Monitoring Compounds 2) 1,3 -Dimethyl -2 -nitrobenzen 13.23 134 936795 3.67 ug/L • 0.00 Spiked Amount 5.000 Recovery 73.40% 19) Triphenyl Phosphate surr 29.69 32 6 1359468 5.30 ug/L 0.00 Spiked Amount 5.000 Recovery = 106.00% 21) Perylene D-12 surr 34.44 264 3066374 4.19 ug/L 0.00 Spiked Amount 5.000 Recovery = 83.80%

Target Compounds Qvalue 3) Hexachlorocyclopentadiene 0.00 237 0 N.D. 4) Hexachlorobenzene 0.00 2 84 0 N.D. 5) EPTC 0.00 128 0 N.D. 6) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 7) 2,4-Dinitotoluene 0.00 165 0 N.D. d 8) Molinate 19.09 12 6 9997 N.D. 10) Simazine 0.00 201 0 N.D. 11) Atrazine 0.00 2 00 0 N.D. 12) Alachlor 0.00 160 0 N.D. 13) Terbacil / 0.00 161 0 N.D. d 14) Acetochlor 0.00 146 0 N.D. 15) Metribuzin 0.00 198 0 N.D. 16) Metolachlor 0.00 162 0 N.D. 17) Butachlor 0.00 160 0 N.D. d 18) 4,4*-DDE 0.00 246 0 ■ : N.D. d 22) Bis (2-Ethylhexyl) adipate 29.62 129 9060 0.12 ug/L # 11 23) Bis (2-Ethylhexyl) phthala 31.07 14 9 120215 0.26 ug/L 100 24) Benzo (a) pyrene 0.00 252 0 N.D. d

(#) = qualifier out of range (m) = manual integration 1116LB.D 120501.M Tue Dec 11 09:13:21 2001 Page 1

NYC-WTC_000057725

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NYC-WTC_000057725Source: NYC Law Department, mirrored locally

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