Laboratory report detailing analysis of sample AD27232 for pesticides and organics using Method 525.
NYC-WTC_000057046–000057048
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)
Data File C:\MSDCHEM\l\DATA\120601\1114LBK.D Vial: 29 Acct On 7 Dec 2001 2:19 pm Operator: McLean Sarple : Inst : Instrumen Mise : Multipir: 1.00 MS Integration Params: BENZO.P Quant Time: Dec 12 11:55:38 2001 Quant Results File: 120501.RES
Quant Method : C:\MSDCHEM\l\5973N\120501.M (RTE Integrator) Title : Quantitation For Method 525.2 Last Update : Thu Dec 06 10:31:04 2001 Response via : Initial Calibration DataAcq Meth : 120501
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) Acenaphthene-diO 18.32 164 3920592 5.00 ug/L 0.00 9) Phenanthrene D-10 22.65 188 6784721 5.00 ug/L 0.00 20) Chrysene D-12 30.43 240 4002597 5.00 ug/L 0.00
System Monitoring Compounds 2) 1,3-Dimethyl-2-nitrobenzen 13.23 134 779452 3.75 ug/L 0.00 Spiked Amount 5.000 Recovery = 75.00% 19) Triphenyl Phosphate surr 29.70 326 1032641 4.39 ug/L 0.01 Spiked Amount 5.000 Recovery = 87.80% 21) Perylene D-12 surr 34.46 264 1717757 3.06 ug/L 0.02 Spiked Amount 5.000 Recovery = 61.20%
Target Compounds Qvalue 3) Hexachlorocyclopentadiene 0.00 237 0 N.D. 4) Hexachlorobenzene 0.00 284 0 N.D. 5) EPTC 0.00 128 0 N.D. 6) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 7) 2,4-Dinitotoluene 0.00 165 0 N.D. d 8) Molinate 19.08 126 7014 N.D. 10) Simazine 0.00 201 0 N.D. 11) Atrazine 0.00 200 0 N.D. 12) Alachlor 0.00 160 0 N.D. 13) Terbacil 0.00 161 0 N.D. d 14) Acetochlor 0.00 146 0 N.D. 15) Metribuzin 0.00 198 0 N.D. 16) Metolachlor 0.00 162 0 N.D. 17) Butachlor 26.77 160 28354 0.10 ug/L # 7 18) 4,4'-DDE 27.52 246 163950 0.58 ug/L # 23 22) Bis (2-Ethylhexyl) adipate 29.62 129 11870 0.13 ug/L # 20 23) Bis (2-Ethylhexyl) phthala 31.07 149 541968 0.70 ug/L 92 24) Benzo (a) pyrene 0.00 252 0 N.D.
(#) = qualifier out of range (m) = manual integration 1114LBK.D 120501.M Wed Dec 12 11:56:22 2001 Page 1
NYC-WTC_000057047
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NYC-WTC_000058063
Laboratory blank analysis results for sample AD28316 showing pesticide compound levels below detection limits on January 17, 2002.
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Laboratory blank analysis results for sample AD28048 showing pesticide compound levels below detection limits on December 18, 2001.
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Laboratory report for sample AD28322 showing non-detects for pesticides and contaminants analyzed on December 19, 2001.
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Quality control report for calibration standards (AD28322) verifying instrument accuracy on December 19, 2001.
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Quality control spiked sample results for Method 525.2 verifying recovery rates for target chemical compounds.
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Record of quality control checks for sample AD28172 performed in January 2002 to verify analytical accuracy.
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Calibration standard analysis results for sample AD28316 showing pesticide compound responses on January 17, 2002.
1 shared topics · Same agency, volume and box · similarity 0.987
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Quality control report for calibration standards (AD28847) verifying instrument accuracy on December 20, 2001.
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Laboratory report listing analytical results for pesticides and organic compounds in calibration standard AD27547.
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Summary of analytical results for sample AD27547 including DDT and Endrin detection data from December 2001.
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Laboratory analysis of reference standard for sample AD27232 using EPA Method 525.2, dated Dec 13, 2001, showing detected levels of pesticides and organic compounds.
1 shared topics · Same agency, volume and box · similarity 0.987
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000055108
Calibration standard reference results for pesticide and organic compound analysis of sample AD27547, with measured values for 13 analytes including hexachlorobenzene (4.96 ug), si
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