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Pesticide analysis method validation data, Dec 2001

Machine-extracted title · confidence 90%

Technical document displaying compound response factors and relative standard deviation for pesticide analysis methods.

NYC-WTC_000056440–000056446

Folder label: “508 X 11/21/01 A 12/20 - 12/21/01

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Scanned page image, NYC-WTC_000056445
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Signal #1 : C:\MSDCHEM\1\DATA\508\011220B\PESTUR.D\ECD1A.CH Vial: 36 Signal #2 : C:\MSDCHEM\1\DATA\508\011220B\PESTUR.D\ECD2B.CH Acq On : 20 Dec 2001 2:28 pm Operator: Nefliu Sample : pest unextracted ref Inst : Instrumen Mise : Multiplr: 1.00 IntFile Signal #1: EVENTS.E IntFile Signal #2: events2.e Quant Time: Jan 08 09:16:23 2002 Quant Results File: 011220P.RES

Quant Method : C:\MSDCHEM\1\METHODS\011220P.M (Chemstation Integrator) Title : 508 Chlorinated Pesticides Last Update : Fri Dec 21 08:18:43 2001 Response via : Initial Calibration DataAcq Meth : MDL508.M

Volume Inj. Signal #1 Phase Signal #2 Phase: Signal #1 Info Signal #2 Info :

Compound RT#1 RT#2 Resp#l Resp#2 ug/l ug/l

System Monitoring Compounds 10) s 2,4-DDD SURROGAT 14.35 14.99 732.6E6 561.2E6 0.198m 0.201 Spiked Amount 0.200 Recovery = 99.00% 100.50%

Target Compounds 1) Propachlor 9.06 8.50 90826093 68130232 0.184 12 0.185 2) g-BHC 9.83 10.19 1190.8E6 862.8E6 0.14507 0.144 3) Heptachlor 11.00 11.24 717.OE6 426.7E6 0.096 0.096 4) 5) Aldrin 11.71 Heptachlor Epoxi 13.15 11.99 13.34 380.5E6 292.OE6 1035.1E6 781.2E6 0.046 0.144 o 2 0.046 0.144 6) 4,4-DDE 13.98 14.55 2674.3E6 2071.8E6 0.39544 0.396 7) Dieldrin 14.56 14.82 552.8E6 434.4E6 0.070m<^'<, 0.075 8) Endrin 15.06 15.47 523.9E6 377.7E6 0.093*13 0.093 9) Methoxychlor 17.00 18.02 422.8E6 231.4E6 0.180 00 0.178

(f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int. PESTUR.D 011220P.M Tue Jan 08 09:16:47 2002 Page 1

NYC-WTC_000056445

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NYC-WTC_000056445Source: NYC Law Department, mirrored locally

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