Second set of calibration verification data for pesticide analysis of sample AD27626 with recovery and detection limits.
NYC-WTC_000055927–000055933Folder label: “508 X 11/16/01 A 12/14/01 - 12/16/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Signal #1 : C:\MSDCHEM\1\DATA\5O8\O11214C\PESTUR.D\ECD1A.CH Vial: 16 Signal #2 : C:\MSDCHEM\l\DATA\508\011214C\PESTUR.D\ECD2B.CH Acq On : 14 Dec 2001 9:29 pm Operator: Nefliu Sample : pest unextracted ref Inst : Instrumen Mise : Multiplr: 1.00 IntFile Signal #1: EVENTS.E IntFile Signal #2: events2.e Quant Time; Dec 27 15:18:29 2001 Quant Results File: 011214P.RES
Quant Method : C:\MSDCHEM\1\METHODS\011214P.M (Chemstation Integrator) Title : 508 Chlorinated Pesticides Last Update : Mon Dec 17 10:51:26 2001 Response via : Initial Calibration DataAcq Meth : MDL508.M
Volume Inj. Signal #1 Phase Signal #2 Phase: Signal #1 Info Signal #2 Info :
Compound RT#1 RT#2 Resp#l Resp#2 ug/1 ug/1
System Monitoring Compounds 10) s 2,4-DDD SURROGAT 14.34 14.97 682.6E6 549.9E6 0.219m 0.195m Spiked Amount 0.200 Recovery = 109.50% 97.50%
Target Compounds 1) Propachlor 9.04 8.49 85387557 71282371 0.178m 81/. 0.191m 2) g-BHC 9.82 10.17 1103.7E6 879.8E6 0.146m49j 0.144m 3) Heptachlor 10.98 11.22 681.6E6 464.4E6 0.098m 08‘ 0.097m 4) Aldrin 11.69 11.97 352.6E6 288.5E6 0.047mqv[. 0.046m 5) Heptachlor Epoxi 13.13 13.33 963.7E6 789.2E6 0.145marl 0.147m 6) 4,4-DDE 13.96 14.54 2536.6E6 2090.3E6 0.401m (08. 2 . 222. 0.403m 7) Dieldrin 14.54 14.80 513.9E6 419.6E6 0.072m90’ 0.074m 8) Endrin 15.04 15.46 475.1E6 384.1E6 0.095mAS/ 0.097m 9) Methoxychlor 16.99 18.01 460.9E6 270.1E6 0.192ma./.0.191m
(f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int. PESTUR.D 011214P.M Thu Jan 03 09:44:32 2002 Page 1
NYC-WTC_000055932
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NYC-WTC_000056440
Technical document displaying compound response factors and relative standard deviation for pesticide analysis methods.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000057180
Calibration data for pesticide analysis using method 508, showing compound response factors.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000055871
Laboratory report listing concentrations of pesticides including Propachlor and Toxaphene in sample AD27776 analyzed via Method 508.
1 shared topics · Same agency, volume and box · similarity 0.986
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089541
Gas chromatography report showing concentrations of multiple pesticides including endrin and heptachlor for sample 508.
1 shared topics · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089991
Raw chromatographic data and compound identification logs for pesticide analysis conducted in December 2001.
1 shared topics · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089831
Technical report displaying calibration data and relative standard deviations for pesticide analysis methods in early 2002.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000092394
Technical document presenting method validation statistics including average response and relative standard deviation for pesticide analysis.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089527
Instrumental analysis report for a reference pesticide sample from December 26, 2001, documenting compound identification and recovery percentages.
1 shared topics · similarity 0.989
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089724
Laboratory report detailing specific pesticide concentrations including Endrin and DDT in environmental sample AD28320 analyzed in late 2001.
1 shared topics · similarity 0.988
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089583
Duplicate calibration verification results for pesticides and PCBs confirming analytical system performance.
1 shared topics · similarity 0.988
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000090012
Laboratory report containing pesticide concentration data and statistical summaries for samples analyzed in December 2001.
1 shared topics · similarity 0.988
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089971
Laboratory report listing pesticide concentrations for sample AD27116 analyzed between November 13 and December 7, 2001.
1 shared topics · similarity 0.986
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000055890
Inspection log or form for site 508 X covering dates in mid-November and mid-December 2001.
Filed in the same folder
NYC-WTC_000055891
Fragmented document page from a DEP environmental monitoring log covering the period of November to December 2001.
Filed in the same folder
NYC-WTC_000055893
Record of laboratory sample extraction and processing parameters including drip rates and pH levels for samples in late 2001.
Filed in the same folder
NYC-WTC_000055895
Computer-generated sequence file listing analytical samples and methods for pesticide testing conducted in December 2001.
Filed in the same folder
NYC-WTC_000055897
Technical log recording instrument status and data acquisition parameters for environmental sample analysis in late 2001.
Filed in the same folder