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Pesticide calibration verification report, sample AD27626

Machine-extracted title · confidence 90%

Second set of calibration verification data for pesticide analysis of sample AD27626 with recovery and detection limits.

NYC-WTC_000055927–000055933

Folder label: “508 X 11/16/01 A 12/14/01 - 12/16/01

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Scanned page image, NYC-WTC_000055930
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Signal #1 : C:\MSDCHEM\1\DATA\5O8\O11214C\PESTC3.D\ECD1A.CH Vial: 15 signal #2 : C:\MSDCHEM\l\DATA\508\011214C\PESTC3.D\ECD2B.CH Acq On : 14 Dec 2001 9:00 pm Operator: Nefliu Sample : pest ic3 Inst : Instrumen Mise : Multiplr: 1.00 IntFile Signal #1: EVENTS.E IntFile Signal #2: events2.e Quant Time: Dec 27 15:05:40 2001 Quant Results File: 011214P.RES

Quant Method : C:\MSDCHEM\1\METHODS\011214P.M (Chemstation Integrator) Title : 508 Chlorinated Pesticides Last Update : Mon Dec 17 10:51:26 2001 Response via : Initial Calibration DataAcq Meth : MDL508.M

Volume Inj. Signal #1 Phase Signal #2 Phase: Signal #1 Info Signal #2 Info :

Compound RT#1 RT#2 Resp#l Resp#2 ug/l ug/l

System Monitoring Compounds 10) s 2,4-DDD SURROGAT 14.34 14.97 678.9E6 535.1E6 0.217m 0.190m Spiked Amount 0.200 Recovery 108.50% 95.00%

Target Compounds 1) Propachlor 9.04 8.49 163.OE6 135.4E6 0.341m 0.362m 2) g-BHC 9.82 10.17 4277.8E6 3510.1E6 0.564m 0.577m 3) Heptachlor 10.99 11.22 1365.8E6 951.1E6 0.195m 0.199m 4) Aldrin 11.69 11.97 1835.9E6 1532.8E6 0.242m 0.247m 5) Heptachlor Epoxi 13.13 13.33 3087.8E6 2555.6E6 0.466m 0.475m 6) 4,4-DDE 13.96 14.54 5010.8E6 4172.2E6 0.792m 0.805m 7) Dieldrin 14.54 14.80 1107.5E6 913.3E6 0.154m 0.160m 8) Endrin 15.04 15.46 2029.9E6 1658.OE6 0.407m 0.417m 9) Methoxychlor 16.99 18.01 1895.2E6 1168.7E6 0.790m 0.827m

(f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int. PESTC3.D 011214P.M Thu Jan 03 09:43:58 2002 Page 1

NYC-WTC_000055930

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NYC-WTC_000055930Source: NYC Law Department, mirrored locally

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