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Method 525 pesticide results, sample AD28324, Dec 2001

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Laboratory report for sample AD28324 showing non-detects for pesticides and contaminants analyzed on December 20, 2001.

NYC-WTC_000055796–000055799

Folder label: “525 X 11/27/01 A 12/17 - 12/18/01

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\MSDCHEM\l\DATA\121701\28324.D Vial: 30 Acq On : 17 Dec 2001 6:31 pm Operator: McLean :;ample : 112701 Inst : Instrumen Misc Multiplr: 1.00 MS Integration Params: BENZO.P Quant Time: Dec 17 19:08:34 2001 Quant Results File: 121401.RES

Quant Method : C:\MSDCHEM\1\5973N\121401.M (RTE Integrator) Title : Quantitation For Method 525.2 Last Update : Mon Dec 17 15:06:05 2001 Response via : Initial Calibration DataAcq Meth : 121401

Internal Standards R.T. Qlon Response Conc Units Dev(Min)

1) Acenaphthene-d10 18.20 164 6927378 5.00 ug/L 0.00 9) Phenanthrene D-10 22.53 188 10682866 5.00 ug/L 0.00 20) Chrysene D-12 30.30 240 7013937 5.00 ug/L 0.00

System Monitoring Compounds 2) 1,3-Dimethyl-2-nitrobenzen 13.13 134 1742307 4.92 ug/L 0.00 Spiked Amount 5.000 Recovery = 98.40% 19) Triphenyl Phosphate surr 29.58 326 1882116 5.79 ug/L 0.00 Spiked Amount 5.000 Recovery = 115.80% 21) Perylene D-12 surr 34.31 264 5104142 5.50 ug/L 0.00 Spiked Amount 5.000 Recovery = 110.00%

Target Compounds Qvalue 3) Hexachlorocyclopentadiene 0.00 237 0 N.D. d 4) Hexachlorobenzene 0.00 284 0 N.D. d 5) EPTC 0.00 128 0 N.D. 6) 2,6-Dinitrotoluene 17.82 165 52020 0.45 ug/L # 34 7) 2,4-Dinitotoluene 0.00 165 0 N.D. d 8) Molinate 0.00 126 0 N.D. d 10) Simazine 0.00 201 0 N.D. d 11) Atrazine 0.00 200 0 N.D. 12) Alachlor 0.00 160 0 N.D. 13) Terbacil 0.00 161 0 N.D. d 14) Acetochlor 23.89 146 7399 0.03 ug/L # 24 15) Metribuzin 0.00 198 0 N.D. 16) Metolachlor 0.00 162 0 N.D. 17) Butachlor 0.00 160 0 N.D. d 18) 4,4'-DDE 27.29 246 19686 0.05 ug/L 86 22) Bis (2-Ethylhexyl) adipate 29.51 129 32576 0.41 ug/L # 1 23) Bis (2-Ethylhexyl) phthala 30.96 149 406021 0.56 ug/L 96 24) Benzo (a) pyrene 0.00 252 0 N.D. d

------------------------------------------------------------------------- (#) = qualifier out of range (m) - manual integration 28324.D 121401.M Wed Dec 19 15:52:59 2001 Page 1

NYC-WTC 000055797

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NYC-WTC_000055797Source: NYC Law Department, mirrored locally

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