Sample AD28046 Method 525.2 analysis, Jan 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\MSDCHEM\1\DATA\012502A\28046RR.D Vial: 11 Acq Gin : 25 Jan 2002 10:10 pm Operator: McLean Sample : REINJ Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.p Quant Time: Jan 25 22:47:14 2002 Quant Results File: 012402DF.RES

Quant Method : C:\MSDCHEM\1\5973N\012402DF.M (RTE Integrator) Title : Quantitation For Method 525.2 Last Update : Tue Dec 04 15:01:26 2001 Response via : Initial Calibration DataAcq Meth : 012402DF

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) Acenaphthene-diO 17.96 164 15070484 5.00 ug/L -0.35 9) Phenanthrene D-10 22.27 188 18902720 5.00 ug/L -0.37 20) Chrysene D-12 30.03 240 12302281 5.00 ug/L -0.39

System Monitoring Compounds 2) 1,3-Dimethyl-2-nitrobenzen 12.89 134 3942343 5.52 ug/L -0.34 Spiked Amount 5.000 Recovery = 110.40% 19) Triphenyl Phosphate 29.33 326 3243244 5.02 ug/L -0.37 Spiked Amount 5.000 Recovery = 100.40% 21) Perylene D-12 34.02 264 7716606 4.35 ug/L -0.42 Spiked Amount 5.000 Recovery = 87.00%

Target Compounds Qvalue 3) Hexachlorocyclopentadiene 15.47 237 15006 0.03 ug/L 94 4) Hexachlorobenzene 21.13 284 31982 0.03 ug/L 93 5) EPTC 15.66 128 5288 N.D. 6) 2,6-Dinitrotoluene 17.81 165 7638 0.01 ug/L 78 7) 2,4-Dinitotoluene 18.70 165 37564 0.05 ug/L 40 8) Molinate 18.89 126 8588 N.D. 10) Simazine 0.00 201 0 N.D. 11) Atrazine 0.00 200 0 N.D. 12) Alachlor 23.30 160 8433 0.01 ug/L # 30 13) Terbacil 22.43 161 9835 0.01 ug/L # 1 14) Acetochlor 23.82 146 5038 N.D. 15) Metribuzin 0.00 198 0 N.D. 16) Metolachlor 24.71 162 6610 N.D. 17) Butachlor 0.00 160 0 N.D. d 18) 4,4'-DDE 27.05 246 17353 0.02 ug/L 92 22) Bis (2-Ethylhexyl) adipate 29.26 129 40507 0.02 ug/L # 1 23) Bis (2-Ethylhexyl) phthala 30.69 149 396923 0.12 ug/L 91 24) Benzo (a) pyrene 33.87 252 16147 N.D.

(#) = qualifier out of range (m) = manual integration 28046RR.D 012402B.M Mon Jan 28 12:21:13 2002 Page 1

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