Calibration standard results for Method 525.2 listing concentrations and detection limits for target compounds.
NYC-WTC_000055380–000055384Folder label: “525 X 11/21/01 A 12/11/01 + REANALYSIS 1/25/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)
Data le : C:\MSDCHEM\l\DATA\012502A\C6.D Vial: 5 Acq On : 25 Jan 2002 12:32 pm Operator: McLean Sample : 5.0 CC Inst : Instrumen Mise ----- - Multiplr: 1.00 MS Integration Params: rteint.p
/gss Quant Time: Jan 25 14:12:08 2002 Quant Results File: 012402B.RES
Quant Method : C:\MSDCHEM\1\5973N\012402B.M (RTE Integrator) Title : Quantitation For Method 525.2 Last Update : Fri Jan 25 11:19:14 2002 Response via : Initial Calibration DataAcq Meth : 012402DF
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) Acenaphthene-diO 17.96 164 13491717 5.00 ug/L 0.00 9) Phenanthrene D-10 22.28 188 15892255 5.00 ug/L 0.00 20) Chrysene D-12 30.03 240 9103069 5.00 ug/L 0.00
System Monitoring Compounds 2) 1,3-Dimethyl-2-nitrobenzen 12.89 134 3540697 5.12 ug/L 0.00 Spiked Amount 5.000 Recovery = 102.40% 19) Triphenyl Phosphate 29.33 326 1910873 3.99 ug/L 0.00 Spiked Amount 5.000 Recovery = 79.80% 21) Perylene D-12 34.03 264 6214108 4.81 ug/L 0.00 Spiked Amount 5.000 Recovery = 96.20%
Target Compounds Qvalue 3) Hexachlorocyclopentadiene 15.47 237 1518173 4.44 ug/L 98 4) Hexachlorobenzene 21.14 284 3888692 4.91 ug/L 98 5) EPTC 15.95 128 6371373 5.28 ug/L 100 6) 2,6-Dinitrotoluene 17.53 165 2363178 4.32 ug/L 97 7) 2,4-Dinitotoluene 18.68 165 2379383 3.89 ug/L 93 8) Molinate 18.85 126 9145532 5.50 ug/L 92 10) Simazine 21.70 201 2095357 4.63 ug/L 99 11) Atrazine 21.82 200 3470469 5.09 ug/L 98 12) Alachlor 23.67 160 3437264 5.28 ug/L 96 13) Terbacil 22.63 161 2496892 4.16 ug/L 99 14) Acetochlor 23.46 146 2319466 5.11 ug/L 95 15) Metribuzin 23.49 198 3131729 4.50 ug/L 97 16) Metolachlor 24.58 162 10343204 5.33 ug/L 97 17) Butachlor 26.41 160 2803086 4.65 ug/L 76 18) 4,4'-DDE 27.04 246 3222865 5.07 ug/L 96 22) Bis (2-Ethylhexyl) adipate 29.27 129 4863970 4.66 ug/L 98 23) Bis (2-Ethylhexyl) phthala 30.70 149 7695348 4.59 ug/L 98 24) Benzo (a) pyrene 33.88 252 7464564 4.47 ug/L 97
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(#) = qualifier out of range (m) = manual integration C6.D 012402B.M Fri Jan 25 14:13:07 2002 Page 1
NYC-WTC_000055383
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NYC-WTC_000055375
Quality control lab blank results for Method 525.2 showing detection limits for various pesticides and contaminants.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000055108
Calibration standard reference results for pesticide and organic compound analysis of sample AD27547, with measured values for 13 analytes including hexachlorobenzene (4.96 ug), si
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000055403
Duplicate spike results for Method 525.2 assessing analytical precision and recovery of spiked compounds.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000055828
Quality control report for calibration standards (AD28322) verifying instrument accuracy on December 19, 2001.
1 shared topics · Same agency, volume and box · similarity 0.990
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000055397
Quality control spiked sample results for Method 525.2 verifying recovery rates for target chemical compounds.
1 shared topics · Same agency, volume and box · similarity 0.989
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000055469
Laboratory results for sample AD28164 analyzing pesticides and organic contaminants using Method 525.2.
1 shared topics · Same agency, volume and box · similarity 0.988
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000055481
Laboratory results for sample AD28167 analyzing pesticides and organic contaminants using Method 525.2.
1 shared topics · Same agency, volume and box · similarity 0.988
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000058028
Laboratory blank analysis results for sample AD28172 showing pesticide compound levels below detection limits on January 16, 2002.
1 shared topics · Same agency, volume and box · similarity 0.988
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000055433
Laboratory results for sample AD28045 analyzing pesticides and organic contaminants using Method 525.2.
1 shared topics · Same agency, volume and box · similarity 0.988
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000055789
Quality control report for calibration standards (AD28324) verifying instrument accuracy on December 20, 2001.
1 shared topics · Same agency, volume and box · similarity 0.988
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000055457
Laboratory results for sample AD28104 analyzing pesticides and organic contaminants using Method 525.2.
1 shared topics · Same agency, volume and box · similarity 0.987
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000055385
Reference standard results for Method 525.2 verifying analytical performance for pesticides and organic compounds.
1 shared topics · Same agency, volume and box · similarity 0.987
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NYC-WTC_000055357
Documentation for a reanalysis of site 525 X samples collected in November 2001 and tested in January 2002.
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Calibration curve and quality control results for Method 525.2 organic compound analysis, showing compound recovery percentages and relative standard deviations.
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Laboratory report detailing chemical compound analysis using Method 525.2 with calibration data and response metrics.
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Laboratory results for sample AD28105 analyzing pesticides including Endrin and DDT using Method 525.2.
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NYC-WTC_000055375
Quality control lab blank results for Method 525.2 showing detection limits for various pesticides and contaminants.
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