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← Document results/DEP Box 30/525 X 11/21/01 A 12/11/01 + REANALYSIS 1/25/02
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Lab blank analysis for Method 525.2, Jan 2002

Machine-extracted title · confidence 100%

Quality control lab blank results for Method 525.2 showing detection limits for various pesticides and contaminants.

NYC-WTC_000055375–000055379

Folder label: “525 X 11/21/01 A 12/11/01 + REANALYSIS 1/25/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File C:\MSDCHEM\1\DATA\012502A\LB1121R.D Vial: 1 Acq On 25 Jan 2002 2:39 pm Operator: McLean Sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.p Quant Time: Jan 28 11:43:32 2002 Quant Results File: 012402B.RES

Quant Method : C:\MSDCHEM\1\5973N\012402B.M (RTE Integrator) Title : Quantitation For Method 525.2 Last Update : Fri Jan 25 11:19:14 2002 Response via : Initial Calibration DataAcq Meth : 012402DF

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) Acenaphthene-diO 17.97 164 15473729 5.00 ug/L 0.00 9) Phenanthrene D-10 22.27 188 20346992 5.00 ug/L 0.00 20) Chrysene D-12 30.03 240 15149429 5.00 ug/L 0.00

System Monitoring Compounds 2) 1,3-Dimethyl-2-nitrobenzen 12.89 134 4018547 5.07 ug/L 0.00 Spiked Amount 5,000 Recovery = 101.40% 19) Triphenyl Phosphate 29.33 326 3137880 5.12 ug/L 0.00 Spiked Amount 5.000 Recovery = 102.40% 21) Perylene D-12 34.03 264 10064447 4.68 ug/L 0.00 Spiked Amount 5.000 Recovery = 93.60%

Target Compounds Qvalue 3) Hexachlorocyclopentadiene 0.00 237 0 N.D. d 4) Hexachlorobenzene 21.14 284 6968 N.D. 5) EPTC 0.00 128 0 N.D. 6) 2,6-Dinitrotoluene 17.60 165 31524 0.86 ug/L 30 7) 2,4-Dinitotoluene 18.70 165 6944 0.91 ug/L 21 8) Molinate 18.90 126 9230 Below Cal # 1 10) Simazine 0.00 201 0 N.D. 11) Atrazine 0.00 200 0 N.D. 12) Alachlor 0.00 160 0 N.D. 13) Terbacil 0.00 161 0 N.D. d 14) Acetochlor 0.00 146 0 N.D. 15) Metribuzin 0.00 198 0 N.D. 16) Metolachlor 0.00 162 0 N.D. d 17) Butachlor 26.38 160 99688 0.46 ug/L 90 18) 4,4'-DDE 0.00 246 0 N.D. d 22) Bis (2-Ethylhexyl) adipate 29.33 129 46679 0.52 ug/L 33 23) Bis (2-Ethylhexyl) phthala 30.69 149 95213 0.40 ug/L 60 24) Benzo (a) pyrene 0.00 252 0 N.D. d

(#) = qualifier out of range (m) = manual integration LB1121R.D 012402B.M Mon Jan 28 11:45:24 2002 Page 1

NYC-WTC_000055378

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NYC-WTC_000055378Source: NYC Law Department, mirrored locally

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